N-(3β,16α-dihydroxy-olean-12-en-28-oyl)-(1-benzyl-1H-1,2,3-triazol-4-yl)-methylamine

Base Information

Chemical Name:N-(3β,16α-dihydroxy-olean-12-en-28-oyl)-(1-benzyl-1H-1,2,3-triazol-4-yl)-methylamine
CAS No.:1601461-19-1
Molecular Formula:C₄₀H₅₈N₄O₃
Molecular Weight:642.926
Hs Code.:

Synonyms:N-(3β,16α-dihydroxy-olean-12-en-28-oyl)-(1-benzyl-1H-1,2,3-triazol-4-yl)-methylamine

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Chemical Property of N-(3β,16α-dihydroxy-olean-12-en-28-oyl)-(1-benzyl-1H-1,2,3-triazol-4-yl)-methylamine

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Technology Process of N-(3β,16α-dihydroxy-olean-12-en-28-oyl)-(1-benzyl-1H-1,2,3-triazol-4-yl)-methylamine

There total 3 articles about N-(3β,16α-dihydroxy-olean-12-en-28-oyl)-(1-benzyl-1H-1,2,3-triazol-4-yl)-methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1438766-95-0
N-propargyl 3β, 16α-dihydroxyolean-12-en-28-amide

: 622-79-7
benzyl azide

: 1601461-19-1
N-(3β,16α-dihydroxy-olean-12-en-28-oyl)-(1-benzyl-1H-1,2,3-triazol-4-yl)-methylamine

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; In dichloromethane; water; at 20 ℃; for 8h;
DOI:10.1016/j.ejmech.2014.03.017

Reference yield:

: 510-30-5
echinocystic acid

: 1601461-19-1
N-(3β,16α-dihydroxy-olean-12-en-28-oyl)-(1-benzyl-1H-1,2,3-triazol-4-yl)-methylamine

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 4 h / 20 °C

2: sodium carbonate / N,N-dimethyl-formamide / 0.33 h / 20 °C

3: copper(II) sulfate; sodium L-ascorbate / dichloromethane; water / 8 h / 20 °C

With sodium carbonate; copper(II) sulfate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.03.017

Reference yield:

: 1438766-88-1
1-benzotriazolyl 3β,16α-dihydroxyolean-12-en-28-oate

: 1601461-19-1
N-(3β,16α-dihydroxy-olean-12-en-28-oyl)-(1-benzyl-1H-1,2,3-triazol-4-yl)-methylamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / N,N-dimethyl-formamide / 0.33 h / 20 °C

2: copper(II) sulfate; sodium L-ascorbate / dichloromethane; water / 8 h / 20 °C

With sodium carbonate; copper(II) sulfate; sodium L-ascorbate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.03.017