(-)-(S)<(dimethyl-2,2 dioxolanne-1,3 yl-4) methyl>-2 dihydroxy-1,4 anthraquinone-9,10

Base Information

Chemical Name:(-)-(S)<(dimethyl-2,2 dioxolanne-1,3 yl-4) methyl>-2 dihydroxy-1,4 anthraquinone-9,10
CAS No.:111301-39-4
Molecular Formula:C₂₀H₁₈O₆
Molecular Weight:354.359
Hs Code.:

Synonyms:(-)-(S)<(dimethyl-2,2 dioxolanne-1,3 yl-4) methyl>-2 dihydroxy-1,4 anthraquinone-9,10

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Chemical Property of (-)-(S)<(dimethyl-2,2 dioxolanne-1,3 yl-4) methyl>-2 dihydroxy-1,4 anthraquinone-9,10

Chemical Property:

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Technology Process of (-)-(S)<(dimethyl-2,2 dioxolanne-1,3 yl-4) methyl>-2 dihydroxy-1,4 anthraquinone-9,10

There total 1 articles about (-)-(S)<(dimethyl-2,2 dioxolanne-1,3 yl-4) methyl>-2 dihydroxy-1,4 anthraquinone-9,10 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 38399-72-3
leuco-1,4-dihydroxyanthraquinone

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 81-64-1,103220-12-8
1,4-dihydroxy-9,10-anthracenedione

: 128885-71-2
dihydroxy-1,4 (hydroxy-3 propyl)-2 anthraquinone-9,10

: 111301-39-4
(-)-(S)<(dimethyl-2,2 dioxolanne-1,3 yl-4) methyl>-2 dihydroxy-1,4 anthraquinone-9,10

: 111301-40-7,111331-26-1
<(dimethyl-2,2 dioxolanne-1,3 yl-4) hydroxymethyl>-2 dihydroxy-1,4 anthraquinone-9,10

Guidance literature:: With potassium hydroxide; sodium hydrogensulfite; Product distribution; 1.) MeOH, 15 min, 20 deg C, 2.) MeOH, 12 h, 20 deg C, further temperatures;

Reference yield:

: 111301-39-4
(-)-(S)<(dimethyl-2,2 dioxolanne-1,3 yl-4) methyl>-2 dihydroxy-1,4 anthraquinone-9,10

: 128885-76-7,128885-77-8,128885-80-3,128885-81-4
nitro-4 benzoate de tridesoxy-2,3,6 O-((dihydroxy-5,12 dioxo-6,11 tetrahydro-3,4,6,11 1H-anthra<2,3-c>pyrannyl-3(S)) methyl)-1 trifluoroacetamido-3 L-lyxo-hexopyrannose

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 0.3 N KOH, sodium bisulfite / 1.) MeOH, 15 min, 2.) H₂O, 20 deg C, 1 h,

2: 20 percent / N-bromosuccinimide, 2,2'-azobis (methyl-2 propionitrile) / CCl₄ / 2 h / Irradiation

3: 30 percent / N HNO₃, AgNO₃ / methanol / 5 h / 20 °C

4: 35 percent / p-toluenesulfonic acid / CH₂Cl₂; benzene / 2 h / 50 °C

With potassium hydroxide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); nitric acid; toluene-4-sulfonic acid; silver nitrate; sodium hydrogensulfite; In methanol; tetrachloromethane; dichloromethane; benzene;

Reference yield:

: 111301-39-4
(-)-(S)<(dimethyl-2,2 dioxolanne-1,3 yl-4) methyl>-2 dihydroxy-1,4 anthraquinone-9,10

: 128885-76-7,128885-77-8,128885-80-3,128885-81-4
Nitro-4 benzoate de Tridesoxy-2,3,6 O-((dihydroxy-5,12 dioxo-6,11 tetrahydro-3,4,6,11 1H-anthra<2,3-c>pyrannyl-3(S)) methyl)-1 trifluoroacetamido-3 L-arabino-hexopyrannose

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 0.3 N KOH, sodium bisulfite / 1.) MeOH, 15 min, 2.) H₂O, 20 deg C, 1 h,

2: 20 percent / N-bromosuccinimide, 2,2'-azobis (methyl-2 propionitrile) / CCl₄ / 2 h / Irradiation

3: 30 percent / N HNO₃, AgNO₃ / methanol / 5 h / 20 °C

4: 26 percent / p-toluenesulfonic acid / benzene; CH₂Cl₂ / 2 h / 50 °C

With potassium hydroxide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); nitric acid; toluene-4-sulfonic acid; silver nitrate; sodium hydrogensulfite; In methanol; tetrachloromethane; dichloromethane; benzene;