tert-butyldiphenyl((19Z,22Z,25Z,28Z,31Z)-12-(phenylsulfonyl)tetratriaconta-19,22,25,28,31-pentaenyloxy)silane-d2

Base Information

• Chemical Name: tert-butyldiphenyl((19Z,22Z,25Z,28Z,31Z)-12-(phenylsulfonyl)tetratriaconta-19,22,25,28,31-pentaenyloxy)silane-d2
• CAS No.: 1260225-85-1
• Molecular Formula: C₅₆H₈₂O₃SSi
• Molecular Weight: 865.401

Synonyms:tert-butyldiphenyl((19Z,22Z,25Z,28Z,31Z)-12-(phenylsulfonyl)tetratriaconta-19,22,25,28,31-pentaenyloxy)silane-d2

Chemical Property of tert-butyldiphenyl((19Z,22Z,25Z,28Z,31Z)-12-(phenylsulfonyl)tetratriaconta-19,22,25,28,31-pentaenyloxy)silane-d2

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Technology Process of tert-butyldiphenyl((19Z,22Z,25Z,28Z,31Z)-12-(phenylsulfonyl)tetratriaconta-19,22,25,28,31-pentaenyloxy)silane-d2

There total 1 articles about tert-butyldiphenyl((19Z,22Z,25Z,28Z,31Z)-12-(phenylsulfonyl)tetratriaconta-19,22,25,28,31-pentaenyloxy)silane-d2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(7Z,10Z,13Z,16Z,19Z)-docosa-7,10,13,16,19-pentaenyl 4-methylbenzenesulfonate-d2 (1260225-83-9) + tert-butyldiphenyl(12-(phenylsulfonyl)dodecyloxy)silane (1260225-80-6) → tert-butyldiphenyl((19Z,22Z,25Z,28Z,31Z)-12-(phenylsulfonyl)tetratriaconta-19,22,25,28,31-pentaenyloxy)silane-d2 (1260225-85-1)

Guidance literature:

tert-butyldiphenyl(12-(phenylsulfonyl)dodecyloxy)silane; With n-butyllithium; In tetrahydrofuran; at -78 - 20 ℃;

(7Z,10Z,13Z,16Z,19Z)-docosa-7,10,13,16,19-pentaenyl 4-methylbenzenesulfonate-d2;

DOI:10.1016/j.tetlet.2010.09.139

Reference yield: 94.0%

tert-butyldiphenyl((19Z,22Z,25Z,28Z,31Z)-12-(phenylsulfonyl)tetratriaconta-19,22,25,28,31-pentaenyloxy)silane-d2 (1260225-85-1) → (19Z,22Z,25Z,28Z,31Z)-12-(phenylsulfonyl)tetratriaconta-19,22,25,28,31-pentaen-1-ol-d2 (1260226-03-6)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran;

DOI:10.1016/j.tetlet.2010.09.139

upstream raw materials:

(7Z,10Z,13Z,16Z,19Z)-docosa-7,10,13,16,19-pentaenyl 4-methylbenzenesulfonate-d2

tert-butyldiphenyl(12-(phenylsulfonyl)dodecyloxy)silane

Downstream raw materials:

(19Z,22Z,25Z,28Z,31Z)-12-(phenylsulfonyl)tetratriaconta-19,22,25,28,31-pentaen-1-ol-d2

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