N-(tert-butoxycarbonyl)-D-tyrosyl-L-valine benzyl ester

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-D-tyrosyl-L-valine benzyl ester
CAS No.:117527-25-0
Molecular Formula:C₂₆H₃₄N₂O₆
Molecular Weight:470.566
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-D-tyrosyl-L-valine benzyl ester

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Chemical Property of N-(tert-butoxycarbonyl)-D-tyrosyl-L-valine benzyl ester

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Technology Process of N-(tert-butoxycarbonyl)-D-tyrosyl-L-valine benzyl ester

There total 1 articles about N-(tert-butoxycarbonyl)-D-tyrosyl-L-valine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 70642-86-3
N-(tert-butoxycarbonyl)-D-tyrosine

: 2462-34-2
L-valine benzyl ester hydrochloride

: 117527-25-0
N-(tert-butoxycarbonyl)-D-tyrosyl-L-valine benzyl ester

Guidance literature:: With diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; at 0 ℃; for 5h;
DOI:10.1021/ja00233a032

Reference yield: 77.0%

: 117527-25-0
N-(tert-butoxycarbonyl)-D-tyrosyl-L-valine benzyl ester

: 117527-26-1
N-(tert-butoxycarbonyl)-D-tyrosyl-L-valine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 1.5h; under 2482.3 Torr;
DOI:10.1021/ja00233a032

Reference yield:

: 117527-25-0
N-(tert-butoxycarbonyl)-D-tyrosyl-L-valine benzyl ester

: N-(tert-butoxycarbonyl)-D-tyrosyl-L-valylglycine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / hydrogen / 5 percent Pd/C / ethyl acetate / 1.5 h / 2482.3 Torr

2: 92 percent / diphenylphosphoryl azid, triethylamine / dimethylformamide / 6 h / 0 °C

With diphenylphosphoranyl azide; hydrogen; triethylamine; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ja00233a032