1,1'-p-xylylbis<4,8,11-tris(tert-butyloxycarbonyl)-1,4,8,11-tetraazacyclotetradecane>

Base Information

Chemical Name:1,1'-p-xylylbis<4,8,11-tris(tert-butyloxycarbonyl)-1,4,8,11-tetraazacyclotetradecane>
CAS No.:175854-48-5
Molecular Formula:C₅₈H₁₀₂N₈O₁₂
Molecular Weight:1103.49
Hs Code.:

Synonyms:1,1'-p-xylylbis<4,8,11-tris(tert-butyloxycarbonyl)-1,4,8,11-tetraazacyclotetradecane>

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Chemical Property of 1,1'-p-xylylbis<4,8,11-tris(tert-butyloxycarbonyl)-1,4,8,11-tetraazacyclotetradecane>

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Technology Process of 1,1'-p-xylylbis<4,8,11-tris(tert-butyloxycarbonyl)-1,4,8,11-tetraazacyclotetradecane>

There total 5 articles about 1,1'-p-xylylbis<4,8,11-tris(tert-butyloxycarbonyl)-1,4,8,11-tetraazacyclotetradecane> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 623-24-5
1,4-bis(bromomethyl)benzene

: 170161-27-0
1,4,8-tris(tert-butoxycarbonyl)-1,4,8,11-tetraazacyclotetradecane

: 175854-48-5
1,1'-p-xylylbis<4,8,11-tris(tert-butyloxycarbonyl)-1,4,8,11-tetraazacyclotetradecane>

Guidance literature:: With sodium carbonate; In acetonitrile; for 48h; Heating;

Reference yield:

: 295-37-4
1,4,8,11-Tetraazacyclotetradecane

: 175854-48-5
1,1'-p-xylylbis<4,8,11-tris(tert-butyloxycarbonyl)-1,4,8,11-tetraazacyclotetradecane>

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / CH₂Cl₂ / 4 h / Ambient temperature

2: 20 percent / K₂CO₃, 5-<4,8-bis(tert-butyloxycarbonyl)-1,4,8,11-tetraazacyclotetradecanyl> pentanoic ethyl ester / acetonitrile / 8 h / Heating

With potassium carbonate; 5-<4,8-bis(tert-butoxycarbonyl)-1,4,8,11-tetraazacyclotetradecanyl>pentanoic ethyl ester; In dichloromethane; acetonitrile;
DOI:10.1021/jm980358u

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 175854-48-5
1,1'-p-xylylbis<4,8,11-tris(tert-butyloxycarbonyl)-1,4,8,11-tetraazacyclotetradecane>

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / CH₂Cl₂ / 4 h / Ambient temperature

2: 20 percent / K₂CO₃, 5-<4,8-bis(tert-butyloxycarbonyl)-1,4,8,11-tetraazacyclotetradecanyl> pentanoic ethyl ester / acetonitrile / 8 h / Heating

With potassium carbonate; 5-<4,8-bis(tert-butoxycarbonyl)-1,4,8,11-tetraazacyclotetradecanyl>pentanoic ethyl ester; In dichloromethane; acetonitrile;
DOI:10.1021/jm980358u