(E)-1-((E)-4-Methoxy-2,3,6,7,8,9-hexahydro-[1,5]diazonin-1-yl)-3-phenyl-propenone

Base Information

Chemical Name:(E)-1-((E)-4-Methoxy-2,3,6,7,8,9-hexahydro-[1,5]diazonin-1-yl)-3-phenyl-propenone
CAS No.:76404-99-4
Molecular Formula:C₁₇H₂₂N₂O₂
Molecular Weight:286.374
Hs Code.:

Synonyms:(E)-1-((E)-4-Methoxy-2,3,6,7,8,9-hexahydro-[1,5]diazonin-1-yl)-3-phenyl-propenone

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Chemical Property of (E)-1-((E)-4-Methoxy-2,3,6,7,8,9-hexahydro-[1,5]diazonin-1-yl)-3-phenyl-propenone

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Technology Process of (E)-1-((E)-4-Methoxy-2,3,6,7,8,9-hexahydro-[1,5]diazonin-1-yl)-3-phenyl-propenone

There total 4 articles about (E)-1-((E)-4-Methoxy-2,3,6,7,8,9-hexahydro-[1,5]diazonin-1-yl)-3-phenyl-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 420-37-1
trimethoxonium tetrafluoroborate

: 76405-00-0
5-[(E)-(3-Phenyl-acryloyl)]-[1,5]diazonan-2-one

: 76404-99-4
(E)-1-((E)-4-Methoxy-2,3,6,7,8,9-hexahydro-[1,5]diazonin-1-yl)-3-phenyl-propenone

Guidance literature:: DOI:10.1246/cl.2000.1104

Reference yield:

: 76405-02-2
[1,5]Diazonan-2-one

: 76404-99-4
(E)-1-((E)-4-Methoxy-2,3,6,7,8,9-hexahydro-[1,5]diazonin-1-yl)-3-phenyl-propenone

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / DMAP / CH₂Cl₂ / 20 °C

2: CH₂Cl₂ / 12 h / 20 °C

With dmap; In dichloromethane;
DOI:10.1016/S0040-4020(02)00731-7

Reference yield:

: 76405-01-1
7-oxo-1,6-diazabicyclo<4.3.0>nonane

: 76404-99-4
(E)-1-((E)-4-Methoxy-2,3,6,7,8,9-hexahydro-[1,5]diazonin-1-yl)-3-phenyl-propenone

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / Na; NH₃ liq. / 1.75 h / -33 °C

2: 95 percent / DMAP / CH₂Cl₂ / 20 °C

3: CH₂Cl₂ / 12 h / 20 °C

With dmap; ammonia; sodium; In dichloromethane;
DOI:10.1016/S0040-4020(02)00731-7