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Technology Process of [Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)](1+)*[B(C6F5)4](1-)=[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)][(B(C6F5)4)]

[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)](1+)*[B(C6F5)4](1-)=[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)][(B(C6F5)4)]

Base Information
  • Chemical Name:[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)](1+)*[B(C6F5)4](1-)=[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)][(B(C6F5)4)]
  • CAS No.:557103-04-5
  • Molecular Formula:C24BF20*C29H66GeNSi3
  • Molecular Weight:1264.74
  • Hs Code.:
[Ge(Si(CH<sub>3</sub>)(C(CH<sub>3</sub>)3)2)3(NCCH<sub>3</sub>)]<sup>(1+)</sup>*[B(C<sub>6</sub>F<sub>5</sub>)4]<sup>(1-)</sup>=[Ge(Si(CH<sub>3</sub>)(C(CH<sub>3</sub>)3)2)3(NCCH<sub>3</sub>)][(B(C<sub>6</sub>F<sub>5</sub>)4)]

Synonyms:[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)](1+)*[B(C6F5)4](1-)=[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)][(B(C6F5)4)]

Suppliers and Price of [Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)](1+)*[B(C6F5)4](1-)=[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)][(B(C6F5)4)]
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Chemical Property of [Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)](1+)*[B(C6F5)4](1-)=[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)][(B(C6F5)4)]
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Technology Process of [Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)](1+)*[B(C6F5)4](1-)=[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)][(B(C6F5)4)]

There total 2 articles about [Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)](1+)*[B(C6F5)4](1-)=[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)][(B(C6F5)4)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

tris[di-tert-butyl(methyl)silyl]germanylium tetrakis(pentafluorophenyl)borate
557103-02-3

tris[di-tert-butyl(methyl)silyl]germanylium tetrakis(pentafluorophenyl)borate

acetonitrile
75-05-8,26809-02-9

acetonitrile

[Ge(Si(CH<sub>3</sub>)(C(CH<sub>3</sub>)3)2)3(NCCH<sub>3</sub>)]<sup>(1+)</sup>*[B(C<sub>6</sub>F<sub>5</sub>)4]<sup>(1-)</sup>=[Ge(Si(CH<sub>3</sub>)(C(CH<sub>3</sub>)3)2)3(NCCH<sub>3</sub>)][(B(C<sub>6</sub>F<sub>5</sub>)4)]
557103-04-5

[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)](1+)*[B(C6F5)4](1-)=[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)][(B(C6F5)4)]

Guidance literature:
In neat (no solvent); dry CH3CN transferred through vac. line to Ge(SiMe(tBu)2)3B(C6F5)4; cooling;
DOI:10.1002/anie.200390300

Reference yield:

tris[di-tert-butyl(methyl)silyl]germyl radical
461054-07-9

tris[di-tert-butyl(methyl)silyl]germyl radical

[Ge(Si(CH<sub>3</sub>)(C(CH<sub>3</sub>)3)2)3(NCCH<sub>3</sub>)]<sup>(1+)</sup>*[B(C<sub>6</sub>F<sub>5</sub>)4]<sup>(1-)</sup>=[Ge(Si(CH<sub>3</sub>)(C(CH<sub>3</sub>)3)2)3(NCCH<sub>3</sub>)][(B(C<sub>6</sub>F<sub>5</sub>)4)]
557103-04-5

[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)](1+)*[B(C6F5)4](1-)=[Ge(Si(CH3)(C(CH3)3)2)3(NCCH3)][(B(C6F5)4)]

Guidance literature:
Multi-step reaction with 2 steps
1: benzene
2: neat (no solvent)
In benzene;
DOI:10.1002/anie.200390300
upstream raw materials:

tris[di-tert-butyl(methyl)silyl]germanylium tetrakis(pentafluorophenyl)borate

acetonitrile

tris[di-tert-butyl(methyl)silyl]germyl radical

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