Tricyclo[3.2.1.02,4]octane-1-carboxylic acid

Base Information

Chemical Name:Tricyclo[3.2.1.02,4]octane-1-carboxylic acid
CAS No.:75444-04-1
Molecular Formula:C₉H₁₂O₂
Molecular Weight:152.193
Hs Code.:
DSSTox Substance ID:DTXSID601183968
Mol file:75444-04-1.mol

Synonyms:75444-04-1;DTXSID601183968;Tricyclo[3.2.1.02,4]octane-1-carboxylic acid, (1alpha,2beta,4beta,5beta)-

Suppliers and Price of Tricyclo[3.2.1.02,4]octane-1-carboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Tricyclo[3.2.1.02,4]octane-1-carboxylic acid

Chemical Property:

PSA：37.30000
LogP:1.50720
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:152.083729621
Heavy Atom Count:11
Complexity:236

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2(CC1C3C2C3)C(=O)O

Technology Process of Tricyclo[3.2.1.02,4]octane-1-carboxylic acid

There total 3 articles about Tricyclo[3.2.1.02,4]octane-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35730-27-9
methyl 1,3-cyclopentadiene-1-carboxylate

: 75444-04-1
endo-Tricyclo<3.2.1.0^2,4>octane-1-carboxylic Acid

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 6 h / -78 °C

2: potassium azodicarboxylate, AcOH / methanol / 1 h

3: aq. NaOH / 3 h / Heating

With potassium diazodicarboxylate; acetic acid; In methanol; sodium hydroxide; diethyl ether;
DOI:10.1021/jo01314a054

Reference yield:

: 75421-03-3
methyl endo-tricyclo<3.2.1.0^2,4>-oct-6-ene-1-carboxylate

: 75444-04-1
endo-Tricyclo<3.2.1.0^2,4>octane-1-carboxylic Acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium azodicarboxylate, AcOH / methanol / 1 h

2: aq. NaOH / 3 h / Heating

With potassium diazodicarboxylate; acetic acid; In methanol; sodium hydroxide;
DOI:10.1021/jo01314a054