Technology Process of C23H22N2O3
There total 4 articles about C23H22N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C28H32N2O6;
With
hydrogenchloride;
In
ethyl acetate;
at 20 ℃;
for 1h;
With
sodium carbonate;
In
ethanol; water;
at 60 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triphenylphosphine; diethylazodicarboxylate / toluene; tetrahydrofuran / 3 h / 20 °C
2.1: potassium carbonate; thiophenol / acetonitrile / 5 h / 20 °C
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / tetrahydrofuran / 18 h / 20 °C
4.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C
4.2: 2 h / 60 °C
With
hydrogenchloride; potassium carbonate; benzotriazol-1-ol; thiophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; ethyl acetate; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate; thiophenol / acetonitrile / 5 h / 20 °C
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / tetrahydrofuran / 18 h / 20 °C
3.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C
3.2: 2 h / 60 °C
With
hydrogenchloride; potassium carbonate; benzotriazol-1-ol; thiophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; ethyl acetate; acetonitrile;
