Technology Process of C16H16Br2N6O3
There total 6 articles about C16H16Br2N6O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridinium hydrobromide perbromide; potassium carbonate;
In
dichloromethane; water;
at 20 ℃;
for 1h;
DOI:10.1002/anie.201102494
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C
2: triethylamine / dichloromethane / 0.5 h / 0 °C
3: potassium cyanide / ethanol / 12 h / 20 °C
4: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
5: pyridinium hydrobromide perbromide; potassium carbonate / dichloromethane; water / 1 h / 20 °C
With
potassium cyanide; tetrabutyl ammonium fluoride; pyridinium hydrobromide perbromide; potassium carbonate; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1002/anie.201102494
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium azide / N,N-dimethyl-formamide / 4.5 h / 20 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C
3: triethylamine / dichloromethane / 0.5 h / 0 °C
4: potassium cyanide / ethanol / 12 h / 20 °C
5: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
6: pyridinium hydrobromide perbromide; potassium carbonate / dichloromethane; water / 1 h / 20 °C
With
potassium cyanide; sodium azide; tetrabutyl ammonium fluoride; pyridinium hydrobromide perbromide; potassium carbonate; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.201102494
