4-(tert-butyl-dimethyl-silanyloxy)-2,2,6,6-tetramethyl-1-(1-phenyl-hex-5-enyloxy)-piperidine

Base Information

Chemical Name:4-(tert-butyl-dimethyl-silanyloxy)-2,2,6,6-tetramethyl-1-(1-phenyl-hex-5-enyloxy)-piperidine
CAS No.:853886-26-7
Molecular Formula:C₂₇H₄₇NO₂Si
Molecular Weight:445.761
Hs Code.:

4-(<i>tert</i>-butyl-dimethyl-silanyloxy)-2,2,6,6-tetramethyl-1-(1-phenyl-hex-5-enyloxy)-piperidine

Synonyms:4-(tert-butyl-dimethyl-silanyloxy)-2,2,6,6-tetramethyl-1-(1-phenyl-hex-5-enyloxy)-piperidine

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Chemical Property of 4-(tert-butyl-dimethyl-silanyloxy)-2,2,6,6-tetramethyl-1-(1-phenyl-hex-5-enyloxy)-piperidine

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Technology Process of 4-(tert-butyl-dimethyl-silanyloxy)-2,2,6,6-tetramethyl-1-(1-phenyl-hex-5-enyloxy)-piperidine

There total 2 articles about 4-(tert-butyl-dimethyl-silanyloxy)-2,2,6,6-tetramethyl-1-(1-phenyl-hex-5-enyloxy)-piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 764638-07-5
4-(tert-butyl-dimethyl-silanyloxy)-2,2,6,6-tetramethyl-piperidin-1-ol

: 38383-05-0
6-bromo-6-phenyl-1-hexene

: 853886-26-7
4-(tert-butyl-dimethyl-silanyloxy)-2,2,6,6-tetramethyl-1-(1-phenyl-hex-5-enyloxy)-piperidine

Guidance literature:: 4-(tert-butyl-dimethyl-silanyloxy)-2,2,6,6-tetramethyl-piperidin-1-ol; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

6-bromo-6-phenyl-1-hexene; In tetrahydrofuran; for 14h; Heating;
DOI:10.1002/chem.200400936

Reference yield:

: 869812-05-5
4-(tert-butyldimethylsilyloxy)-2,2,6,6-tetramethylpiperidinyloxy

: 853886-26-7
4-(tert-butyl-dimethyl-silanyloxy)-2,2,6,6-tetramethyl-1-(1-phenyl-hex-5-enyloxy)-piperidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. calcium ascorbate / 0.25 h / 20 °C

2.1: NaH / tetrahydrofuran / 0.5 h / 20 °C

2.2: 493 mg / tetrahydrofuran / 14 h / Heating

With sodium hydride; L-ascorbic acid calcium salt; In tetrahydrofuran;
DOI:10.1002/chem.200400936