C₆H₅C(CH₂NSi(CH₃)3)3TiBr

Base Information

Chemical Name:C₆H₅C(CH₂NSi(CH₃)3)3TiBr
CAS No.:176248-90-1
Molecular Formula:C₁₉H₃₈BrN₃Si₃Ti
Molecular Weight:520.571
Hs Code.:

C<sub>6</sub>H<sub>5</sub>C(CH<sub>2</sub>NSi(CH<sub>3</sub>)3)3TiBr

Synonyms:C₆H₅C(CH₂NSi(CH₃)3)3TiBr

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Chemical Property of C₆H₅C(CH₂NSi(CH₃)3)3TiBr

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Technology Process of C₆H₅C(CH₂NSi(CH₃)3)3TiBr

There total 1 articles about C₆H₅C(CH₂NSi(CH₃)3)3TiBr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 60864-10-0
TiBr₄(THF)2

: 162463-17-4
α,α,α-tris<<(trimethylsilyl)amino>methyl>toluene

: 176248-90-1
C₆H₅C(CH₂NSi(CH₃)3)3TiBr

Guidance literature:: With BuLi; In pentane; byproducts: LiCl; Ar-atmosphere; addn. of BuLi (in hexanes) to ligand (in pentane) at -40°C, warming to room temp., refluxing for 10 min, addn. of Ti-complex (at -55°C), warming to room temp. over 20 h; filtration, solvent removal (0.001 Torr); cont. 5% impurities;

Reference yield: 41.0%

: K{Ru(η5-C5H5)(CO)2}

: 176248-90-1
C₆H₅C(CH₂NSi(CH₃)3)3TiBr

: C₆H₅C(CH₂NSi(CH₃)3)3TiRu(CO)2(C₅H₅)

Guidance literature:: In toluene; Ar-atmosphere; addn. of 1 equiv. metal carbonylate to Ti-complex at -70°C, warming to room temp. over 20 h; evapn., extn. into pentane, filtration, evapn., washing (cold pentane); elem. anal.;

Reference yield: 32.0%

: potassium cyclopentadienyldicarbonyliron⁽⁰⁾

: 176248-90-1
C₆H₅C(CH₂NSi(CH₃)3)3TiBr

: C₆H₅C(CH₂NSi(CH₃)3)3TiFe(CO)2(C₅H₅)

Guidance literature:: In toluene; Ar-atmosphere; addn. of 1 equiv. metal carbonylate to Ti-complex at -70°C, warming to room temp. over 20 h; evapn., extn. into pentane, filtration, evapn., washing (cold pentane); elem. anal.;