Technology Process of C17H28N2O3S
There total 3 articles about C17H28N2O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
heptanal; 3-azido-N-tosylpropan-1-amine;
With
trifluorormethanesulfonic acid;
In
dichloromethane;
at 20 ℃;
for 1h;
With
potassium hydroxide;
In
dichloromethane; water;
for 1h;
DOI:10.1021/ol400213f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine; dmap / dichloromethane / 0.33 h / 20 °C
2.1: sodium azide; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 36 h / 20 °C
3.1: trifluorormethanesulfonic acid / dichloromethane / 1 h / 20 °C
3.2: 1 h
With
dmap; sodium azide; trifluorormethanesulfonic acid; tetra-(n-butyl)ammonium iodide; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
3.1: |Schmidt Reaction;
DOI:10.1021/ol400213f
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium azide; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 36 h / 20 °C
2.1: trifluorormethanesulfonic acid / dichloromethane / 1 h / 20 °C
2.2: 1 h
With
sodium azide; trifluorormethanesulfonic acid; tetra-(n-butyl)ammonium iodide;
In
dichloromethane; N,N-dimethyl-formamide;
2.1: |Schmidt Reaction;
DOI:10.1021/ol400213f