1-(tert-butoxycarbonyl)-4-({[4-(2-butynyloxy)phenyl]sulfonyl} amino)-4-piperidinecarboxylic acid

Base Information

Chemical Name:1-(tert-butoxycarbonyl)-4-({[4-(2-butynyloxy)phenyl]sulfonyl} amino)-4-piperidinecarboxylic acid
CAS No.:287408-73-5
Molecular Formula:C₂₁H₂₈N₂O₇S
Molecular Weight:452.529
Hs Code.:

Synonyms:1-(tert-butoxycarbonyl)-4-({[4-(2-butynyloxy)phenyl]sulfonyl} amino)-4-piperidinecarboxylic acid

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Chemical Property of 1-(tert-butoxycarbonyl)-4-({[4-(2-butynyloxy)phenyl]sulfonyl} amino)-4-piperidinecarboxylic acid

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Technology Process of 1-(tert-butoxycarbonyl)-4-({[4-(2-butynyloxy)phenyl]sulfonyl} amino)-4-piperidinecarboxylic acid

There total 2 articles about 1-(tert-butoxycarbonyl)-4-({[4-(2-butynyloxy)phenyl]sulfonyl} amino)-4-piperidinecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 183673-71-4
4-amino-1-(tert-butoxycarbonyl)piperidine-4-carboxylic acid

: 286459-94-7
4-but-2-ynyloxybenzenesulfonyl chloride

: 287408-73-5
1-(tert-butoxycarbonyl)-4-({[4-(2-butynyloxy)phenyl]sulfonyl} amino)-4-piperidinecarboxylic acid

Guidance literature:: With hydrogenchloride; sodium hydroxide; triethylamine; In 1,4-dioxane; water; ethyl acetate;

Reference yield:

: C₁₆H₁₈ClNO₄S₂

: 183673-71-4
4-amino-1-(tert-butoxycarbonyl)piperidine-4-carboxylic acid

: 286459-94-7
4-but-2-ynyloxybenzenesulfonyl chloride

: 287408-73-5
1-(tert-butoxycarbonyl)-4-({[4-(2-butynyloxy)phenyl]sulfonyl} amino)-4-piperidinecarboxylic acid

Guidance literature:: 4-amino-1-(tert-butoxycarbonyl)piperidine-4-carboxylic acid; 4-but-2-ynyloxybenzenesulfonyl chloride; With sodium hydroxide; triethylamine; In 1,4-dioxane; water; for 40h;

C₁₆H₁₈ClNO₄S₂; With hydrogenchloride; In 1,4-dioxane; water; ethyl acetate;

Reference yield:

: 287408-73-5
1-(tert-butoxycarbonyl)-4-({[4-(2-butynyloxy)phenyl]sulfonyl} amino)-4-piperidinecarboxylic acid

: C₂₁H₂₇ClN₂O₆S

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 ℃; for 0.25h;

1-(tert-butoxycarbonyl)-4-({[4-(2-butynyloxy)phenyl]sulfonyl} amino)-4-piperidinecarboxylic acid; In DMF (N,N-dimethyl-formamide); dichloromethane; at 20 ℃; for 1h;