C₃₃H₅₃BrO₄Si₂

Base Information

Chemical Name:C₃₃H₅₃BrO₄Si₂
CAS No.:1266178-99-7
Molecular Formula:C₃₃H₅₃BrO₄Si₂
Molecular Weight:649.856
Hs Code.:

C<sub>33</sub>H<sub>53</sub>BrO<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₃H₅₃BrO₄Si₂

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Chemical Property of C₃₃H₅₃BrO₄Si₂

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Technology Process of C₃₃H₅₃BrO₄Si₂

There total 5 articles about C₃₃H₅₃BrO₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1266178-34-0
C₃₉H₆₇BrO₄Si₃

: 1266178-99-7
C₃₃H₅₃BrO₄Si₂

Guidance literature:: With trichloroacetic acid; In tetrahydrofuran; water; chemoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201005850

Reference yield:

: C₃₀H₄₆O₃Si₂

: 1266178-99-7
C₃₃H₅₃BrO₄Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: silver nitrate; calcium carbonate / water; acetone / 4 h / Inert atmosphere; Darkness

2: N-Bromosuccinimide; water / 48 h / 10 °C / Inert atmosphere; Darkness

3: water; sodium hydrogencarbonate / methanol / Inert atmosphere

4: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

5: trichloroacetic acid / tetrahydrofuran; water / Inert atmosphere

With 2,6-dimethylpyridine; N-Bromosuccinimide; water; sodium hydrogencarbonate; silver nitrate; calcium carbonate; trichloroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1002/anie.201005850

Reference yield:

: 1266178-31-7
C₃₀H₄₆O₃Si₂

: 1266178-99-7
C₃₃H₅₃BrO₄Si₂

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide; water / 48 h / 10 °C / Inert atmosphere; Darkness

2: water; sodium hydrogencarbonate / methanol / Inert atmosphere

3: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

4: trichloroacetic acid / tetrahydrofuran; water / Inert atmosphere

With 2,6-dimethylpyridine; N-Bromosuccinimide; water; sodium hydrogencarbonate; trichloroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/anie.201005850