Technology Process of C28H30O6
There total 9 articles about C28H30O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
tetrahydrofuran;
at 80 ℃;
for 9h;
DOI:10.1248/cpb.28.2468
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 66 percent / sodium amide / tetrahydrofuran; liquid ammonia / 2 h / -78 °C
2: 60 percent / sodium / tetrahydrofuran; liquid ammonia / 0.83 h / -78 °C
3: 78.3 percent / NaH (50 percent oil dispersion) / tetrahydrofuran / 15 h / Heating
4: 85.7 percent / 10 percent aq. hydrochloric acid / tetrahydrofuran / 4 h / Ambient temperature
5: sodium hydride (50 percent oil dispersion) / benzene / 0.5 h / Ambient temperature
6: benzene / 1 h / Ambient temperature
7: 41 percent / various solvent(s) / 15 h / 190 °C
8: 53 percent / 10 percent hydrochloric acid / tetrahydrofuran / 9 h / 80 °C
With
hydrogenchloride; sodium; sodium hydride; sodium amide;
In
tetrahydrofuran; ammonia; benzene;
DOI:10.1248/cpb.28.2468
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 66 percent / sodium amide / tetrahydrofuran; liquid ammonia / 2 h / -78 °C
2: 60 percent / sodium / tetrahydrofuran; liquid ammonia / 0.83 h / -78 °C
3: 78.3 percent / NaH (50 percent oil dispersion) / tetrahydrofuran / 15 h / Heating
4: 85.7 percent / 10 percent aq. hydrochloric acid / tetrahydrofuran / 4 h / Ambient temperature
5: sodium hydride (50 percent oil dispersion) / benzene / 0.5 h / Ambient temperature
6: benzene / 1 h / Ambient temperature
7: 41 percent / various solvent(s) / 15 h / 190 °C
8: 53 percent / 10 percent hydrochloric acid / tetrahydrofuran / 9 h / 80 °C
With
hydrogenchloride; sodium; sodium hydride; sodium amide;
In
tetrahydrofuran; ammonia; benzene;
DOI:10.1248/cpb.28.2468
