benzyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-1H-benzindol-1-yl)carbonyl>benzoate

Base Information

• Chemical Name: benzyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-1H-benzindol-1-yl)carbonyl>benzoate
• CAS No.: 121866-12-4
• Molecular Formula: C₃₁H₃₁NO₃
• Molecular Weight: 465.592

Synonyms:benzyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-1H-benzindol-1-yl)carbonyl>benzoate

Chemical Property of benzyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-1H-benzindol-1-yl)carbonyl>benzoate

Chemical Property:

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Technology Process of benzyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-1H-benzindol-1-yl)carbonyl>benzoate

There total 3 articles about benzyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-1H-benzindol-1-yl)carbonyl>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-3-nitronaphthalen-2-yl)ethanal semicarbazone (121866-10-2) → benzyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-1H-benzindol-1-yl)carbonyl>benzoate (121866-12-4)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C

2: 1) NaH / 1) DMF, 1 h, 2) 0 deg C, 3 h

With hydrogen; sodium hydride; palladium on activated charcoal;

DOI:10.1021/jm00130a011

Reference yield:

1,2,3,4-tetrahydro-1,1,4,4,6-pentamethyl-7-nitronaphthalene (116233-16-0) → benzyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-1H-benzindol-1-yl)carbonyl>benzoate (121866-12-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 1) DMF, 115 deg C, 24 h, 2) H₂O, r.t., 20 min

2: H₂ / 10percent Pd/C

3: 1) NaH / 1) DMF, 1 h, 2) 0 deg C, 3 h

With hydrogen; sodium hydride; palladium on activated charcoal;

DOI:10.1021/jm00130a011

Reference yield:

4-benzyloxycarbonyl-benzoyl chloride (67852-95-3) + 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-1H-benzindole (121866-11-3) → benzyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-1H-benzindol-1-yl)carbonyl>benzoate (121866-12-4)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1) DMF, 1 h, 2) 0 deg C, 3 h;

DOI:10.1021/jm00130a011

upstream raw materials:

4-benzyloxycarbonyl-benzoyl chloride

5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-1H-benzindole

2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-3-nitronaphthalen-2-yl)ethanal semicarbazone

1,2,3,4-tetrahydro-1,1,4,4,6-pentamethyl-7-nitronaphthalene

Downstream raw materials:

4-[(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-1H-benz[f]indol-1-yl)carbonyl]benzoic acid

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