cis-Cyclobutane-1,2-diylbis<(methyleneoxy)triphenylphosphonium triflate>

Base Information

Chemical Name:cis-Cyclobutane-1,2-diylbis<(methyleneoxy)triphenylphosphonium triflate>
CAS No.:77774-09-5
Molecular Formula:2CF₃O₃S*C₄₂H₄₀O₂P₂
Molecular Weight:936.867
Hs Code.:

Synonyms:cis-Cyclobutane-1,2-diylbis<(methyleneoxy)triphenylphosphonium triflate>

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Chemical Property of cis-Cyclobutane-1,2-diylbis<(methyleneoxy)triphenylphosphonium triflate>

Chemical Property:

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Technology Process of cis-Cyclobutane-1,2-diylbis<(methyleneoxy)triphenylphosphonium triflate>

There total 2 articles about cis-Cyclobutane-1,2-diylbis<(methyleneoxy)triphenylphosphonium triflate> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 54445-64-6
(1R,2S)-(2-hydroxymethylcyclobutyl)methanol

: 603-35-0
triphenylphosphine

: 77774-09-5
cis-Cyclobutane-1,2-diylbis<(methyleneoxy)triphenylphosphonium triflate>

: 791-28-6
Triphenylphosphine oxide

Guidance literature:: In dichloromethane;
DOI:10.1021/jo00330a031

Reference yield:

: 77774-01-7,446840-28-4
(1R,4S)-(4-hydroxymethylcyclobut-2-enyl)methanol

: 77774-09-5
cis-Cyclobutane-1,2-diylbis<(methyleneoxy)triphenylphosphonium triflate>

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / ethyl acetate

2: CH₂Cl₂

With hydrogen; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jo00330a031