Technology Process of C46H29N3S
There total 8 articles about C46H29N3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
N,N-dimethyl-formamide;
for 1h;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 24h;
- Guidance literature:
-
With
potassium phosphate; tetrakis(triphenylphosphine) palladium(0);
In
ethanol; water; toluene;
for 4h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethyl phosphite / 1,2-dichloro-benzene / 5 h / 150 °C
2.1: copper(l) iodide; potassium phosphate; ethylenediamine / toluene / 15 h / Reflux
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C
3.2: 5 h / -78 - 20 °C
4.1: tetrakis(triphenylphosphine) palladium(0); potassium phosphate / toluene; ethanol; water / 4 h / Reflux
With
potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; ethylenediamine; triethyl phosphite;
In
tetrahydrofuran; ethanol; hexane; water; 1,2-dichloro-benzene; toluene;