1,3-dihydro-1,3-dimesityl-2-selena-1-phospha-3-boraphenalene-1-selenide

Base Information

Chemical Name:1,3-dihydro-1,3-dimesityl-2-selena-1-phospha-3-boraphenalene-1-selenide
CAS No.:1601492-58-3
Molecular Formula:C₂₈H₂₈BPSe₂
Molecular Weight:564.235
Hs Code.:

Synonyms:1,3-dihydro-1,3-dimesityl-2-selena-1-phospha-3-boraphenalene-1-selenide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-dihydro-1,3-dimesityl-2-selena-1-phospha-3-boraphenalene-1-selenide

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Technology Process of 1,3-dihydro-1,3-dimesityl-2-selena-1-phospha-3-boraphenalene-1-selenide

There total 8 articles about 1,3-dihydro-1,3-dimesityl-2-selena-1-phospha-3-boraphenalene-1-selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1601492-55-0
1,3-dihydro-1,3-dimesityl-2-selena-1-phospha-3-boraphenalene

: 1601492-58-3
1,3-dihydro-1,3-dimesityl-2-selena-1-phospha-3-boraphenalene-1-selenide

Guidance literature:: With selenium; In benzene-d6; at 100 ℃; for 84h; Inert atmosphere; Sealed tube;
DOI:10.1002/chem.201304644

Reference yield: 54.0%

: 7782-49-2
selenium

: 1352730-79-0
1,2-dimesityl-1-phospha-2-boraacenaphthene

: 1601492-55-0
1,3-dihydro-1,3-dimesityl-2-selena-1-phospha-3-boraphenalene

: 1601492-58-3
1,3-dihydro-1,3-dimesityl-2-selena-1-phospha-3-boraphenalene-1-selenide

Guidance literature:: In benzene-d6; at 100 ℃; for 120h; Inert atmosphere; Sealed tube;
DOI:10.1002/chem.201304644

Reference yield:

: 1352730-80-3
1-dichlorophosphino-8-dimesitylborylnaphthalene

: 1601492-58-3
1,3-dihydro-1,3-dimesityl-2-selena-1-phospha-3-boraphenalene-1-selenide

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium / tetrahydrofuran / 20 °C / Sealed tube; Inert atmosphere

2.1: benzene-d6 / 120 h / 100 °C / Inert atmosphere; Sealed tube

3.1: benzene-d6 / 19 h / 80 °C / Inert atmosphere; Sealed tube

3.2: 120 h / 100 °C / Inert atmosphere; Sealed tube

With magnesium; In tetrahydrofuran; benzene-d6;
DOI:10.1002/chem.201304644