ethyl 4-(3,5-dimethyl-4-(2-(2,4-dimethylthiophen-3-yl)-3,3,4,4,5,5-hexafluoro-cyclopent-1-enyl)thiophen-2-yl)benzoate

Base Information

• Chemical Name: ethyl 4-(3,5-dimethyl-4-(2-(2,4-dimethylthiophen-3-yl)-3,3,4,4,5,5-hexafluoro-cyclopent-1-enyl)thiophen-2-yl)benzoate
• CAS No.: 1004751-31-8
• Molecular Formula: C₂₆H₂₂F₆O₂S₂
• Molecular Weight: 544.582

Synonyms:ethyl 4-(3,5-dimethyl-4-(2-(2,4-dimethylthiophen-3-yl)-3,3,4,4,5,5-hexafluoro-cyclopent-1-enyl)thiophen-2-yl)benzoate

Chemical Property of ethyl 4-(3,5-dimethyl-4-(2-(2,4-dimethylthiophen-3-yl)-3,3,4,4,5,5-hexafluoro-cyclopent-1-enyl)thiophen-2-yl)benzoate

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Technology Process of ethyl 4-(3,5-dimethyl-4-(2-(2,4-dimethylthiophen-3-yl)-3,3,4,4,5,5-hexafluoro-cyclopent-1-enyl)thiophen-2-yl)benzoate

There total 1 articles about ethyl 4-(3,5-dimethyl-4-(2-(2,4-dimethylthiophen-3-yl)-3,3,4,4,5,5-hexafluoro-cyclopent-1-enyl)thiophen-2-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

2-(4-(3,3,4,4,5,5-hexafluoro-2-(2,4-dimethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiophen-3-yl)cyclopent-1-enyl)-3,5-dimethylthiophen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1004751-30-7) + Ethyl 4-bromobenzoate (5798-75-4) → ethyl 4-(3,5-dimethyl-4-(2-(2,4-dimethylthiophen-3-yl)-3,3,4,4,5,5-hexafluoro-cyclopent-1-enyl)thiophen-2-yl)benzoate (1004751-31-8)

Guidance literature:

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 23h; Heating;

DOI:10.1039/b713663c

Reference yield: 80.0%

ethyl 4-(3,5-dimethyl-4-(2-(2,4-dimethylthiophen-3-yl)-3,3,4,4,5,5-hexafluoro-cyclopent-1-enyl)thiophen-2-yl)benzoate (1004751-31-8) → ethyl 4-(4-(2-(5-bromo-2,4-dimethylthiophen-3-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl)-3,5-dimethylthiophen-2-yl)benzoate (1004751-32-9)

Guidance literature:

With N-Bromosuccinimide; In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1039/b713663c

upstream raw materials:

2-(4-(3,3,4,4,5,5-hexafluoro-2-(2,4-dimethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiophen-3-yl)cyclopent-1-enyl)-3,5-dimethylthiophen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Ethyl 4-bromobenzoate

Downstream raw materials:

ethyl 4-(4-(2-(5-bromo-2,4-dimethylthiophen-3-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl)-3,5-dimethylthiophen-2-yl)benzoate

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