(2S)-2-benzyloxycarbonylamino-5-((1-methoxycarbonylmethyl)cyclohexyl)pentanoic acid benzyl ester

Base Information

Chemical Name:(2S)-2-benzyloxycarbonylamino-5-((1-methoxycarbonylmethyl)cyclohexyl)pentanoic acid benzyl ester
CAS No.:855527-20-7
Molecular Formula:C₂₉H₃₇NO₆
Molecular Weight:495.616
Hs Code.:

Synonyms:(2S)-2-benzyloxycarbonylamino-5-((1-methoxycarbonylmethyl)cyclohexyl)pentanoic acid benzyl ester

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Chemical Property of (2S)-2-benzyloxycarbonylamino-5-((1-methoxycarbonylmethyl)cyclohexyl)pentanoic acid benzyl ester

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Technology Process of (2S)-2-benzyloxycarbonylamino-5-((1-methoxycarbonylmethyl)cyclohexyl)pentanoic acid benzyl ester

There total 5 articles about (2S)-2-benzyloxycarbonylamino-5-((1-methoxycarbonylmethyl)cyclohexyl)pentanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 855527-19-4
(2S)-2-benzyloxycarbonylamino-5-((1-methoxycarbonylmethylcyclohexyl)acetylperoxy)-5-oxopentanoic acid benzyl ester

: 855527-20-7
(2S)-2-benzyloxycarbonylamino-5-((1-methoxycarbonylmethyl)cyclohexyl)pentanoic acid benzyl ester

Guidance literature:: at -78 ℃; for 36h; UV-irradiation;
DOI:10.1021/jo050539l

Reference yield:

: 855527-18-3
(1-hydroperoxycarbonylmethylcyclohexyl)acetic acid methyl ester

: 855527-20-7
(2S)-2-benzyloxycarbonylamino-5-((1-methoxycarbonylmethyl)cyclohexyl)pentanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / dicyclohexyldicarboximide / CH₂Cl₂ / 0 - 20 °C

2: 34 percent / 36 h / -78 °C / UV-irradiation

With dicyclohexyldicarboximide; In dichloromethane;
DOI:10.1021/jo050539l

Reference yield:

: 4355-11-7
1,1-cyclohexanediacetic acid

: 855527-20-7
(2S)-2-benzyloxycarbonylamino-5-((1-methoxycarbonylmethyl)cyclohexyl)pentanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: acetyl chloride / 3 h / 60 °C

2: 6.27 g / methanol / 12 h / Heating

3: 78 percent / H₂SO₄; H₂O₂ / H₂O / 0 - 20 °C

4: 80 percent / dicyclohexyldicarboximide / CH₂Cl₂ / 0 - 20 °C

5: 34 percent / 36 h / -78 °C / UV-irradiation

With dicyclohexyldicarboximide; sulfuric acid; dihydrogen peroxide; acetyl chloride; In methanol; dichloromethane; water;
DOI:10.1021/jo050539l