10,11-Dihydro-2,3-dimethoxy-11-<(2-methoxyphenoxy)-methyl>-5,10-o-benzeno-5H-dibenzocycloheptene

Base Information

Chemical Name:10,11-Dihydro-2,3-dimethoxy-11-<(2-methoxyphenoxy)-methyl>-5,10-o-benzeno-5H-dibenzocycloheptene
CAS No.:84064-74-4
Molecular Formula:C₃₁H₂₈O₄
Molecular Weight:464.561
Hs Code.:

10,11-Dihydro-2,3-dimethoxy-11-<(2-methoxyphenoxy)-methyl>-5,10-o-benzeno-5H-dibenzo<a,d>cycloheptene

Synonyms:10,11-Dihydro-2,3-dimethoxy-11-<(2-methoxyphenoxy)-methyl>-5,10-o-benzeno-5H-dibenzocycloheptene

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Chemical Property of 10,11-Dihydro-2,3-dimethoxy-11-<(2-methoxyphenoxy)-methyl>-5,10-o-benzeno-5H-dibenzocycloheptene

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Technology Process of 10,11-Dihydro-2,3-dimethoxy-11-<(2-methoxyphenoxy)-methyl>-5,10-o-benzeno-5H-dibenzocycloheptene

There total 2 articles about 10,11-Dihydro-2,3-dimethoxy-11-<(2-methoxyphenoxy)-methyl>-5,10-o-benzeno-5H-dibenzocycloheptene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 84107-45-9,74838-68-9
1-(3,4-Dimethoxyphenyl)-1-(9-hydroxyanthracen-10-yl)-2-(2-methoxyphenoxy)ethane

: 84064-74-4
10,11-Dihydro-2,3-dimethoxy-11-<(2-methoxyphenoxy)-methyl>-5,10-o-benzeno-5H-dibenzocycloheptene

Guidance literature:: With boron trifluoride diethyl etherate; In acetic acid; for 24h; Ambient temperature;
DOI:10.1021/jo00151a018

Reference yield:

: 74838-66-7
10-[(S)-1-(3,4-Dimethoxy-phenyl)-2-(2-methoxy-phenoxy)-ethyl]-10H-anthracen-9-one

: 84064-74-4
10,11-Dihydro-2,3-dimethoxy-11-<(2-methoxyphenoxy)-methyl>-5,10-o-benzeno-5H-dibenzocycloheptene

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / LiAlH₄ / tetrahydrofuran / 12 h / Ambient temperature; or reflux, 1 h

2: 72 percent / BF₃*Et₂O / acetic acid / 24 h / Ambient temperature

With lithium aluminium tetrahydride; boron trifluoride diethyl etherate; In tetrahydrofuran; acetic acid;
DOI:10.1021/jo00151a018