6’-[bis(2-pyridylmethyl)aminomethyl]-5-(4-methoxyphenyl)-2,2’-bipyridine

Base Information

Chemical Name:6’-[bis(2-pyridylmethyl)aminomethyl]-5-(4-methoxyphenyl)-2,2’-bipyridine
CAS No.:1404197-76-7
Molecular Formula:C₃₀H₂₇N₅O
Molecular Weight:473.577
Hs Code.:

Synonyms:6’-[bis(2-pyridylmethyl)aminomethyl]-5-(4-methoxyphenyl)-2,2’-bipyridine

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Chemical Property of 6’-[bis(2-pyridylmethyl)aminomethyl]-5-(4-methoxyphenyl)-2,2’-bipyridine

Chemical Property:

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Technology Process of 6’-[bis(2-pyridylmethyl)aminomethyl]-5-(4-methoxyphenyl)-2,2’-bipyridine

There total 3 articles about 6’-[bis(2-pyridylmethyl)aminomethyl]-5-(4-methoxyphenyl)-2,2’-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1263369-01-2
5-(4-methoxyphenyl)-6'-bromomethyl-2,2'-bipyridine

: 1539-42-0
bis[(2-pyridyl)methyl]amine

: 1404197-76-7
6’-[bis(2-pyridylmethyl)aminomethyl]-5-(4-methoxyphenyl)-2,2’-bipyridine

Guidance literature:: With potassium carbonate; In acetonitrile; for 12h; Reflux;
DOI:10.1016/j.tetlet.2012.09.027

Reference yield:

: 1263368-94-0
5-(4-methoxyphenyl)-6'-methoxycarbonyl-2,2'-bipyridine

: 1404197-76-7
6’-[bis(2-pyridylmethyl)aminomethyl]-5-(4-methoxyphenyl)-2,2’-bipyridine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / ethanol / 2 h / Reflux

2: phosphorus tribromide / dichloromethane / 8 h

3: potassium carbonate / acetonitrile / 12 h / Reflux

With sodium tetrahydroborate; phosphorus tribromide; potassium carbonate; In ethanol; dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2012.09.027

Reference yield:

: 1263368-89-3
methyl 6-[6-(4-methoxyphenyl)-1,2,4-triazin-3-yl]pyridine-2-carboxylate

: 1404197-76-7
6’-[bis(2-pyridylmethyl)aminomethyl]-5-(4-methoxyphenyl)-2,2’-bipyridine

Guidance literature:: Multi-step reaction with 4 steps

1: o-xylene / 48 h / Reflux

2: sodium tetrahydroborate / ethanol / 2 h / Reflux

3: phosphorus tribromide / dichloromethane / 8 h

4: potassium carbonate / acetonitrile / 12 h / Reflux

With sodium tetrahydroborate; phosphorus tribromide; potassium carbonate; In ethanol; dichloromethane; o-xylene; acetonitrile;
DOI:10.1016/j.tetlet.2012.09.027