3-methyl-5-[2-({[4-(methyloxy)phenyl]methyl}oxy)phenyl]-2-(5-methyl-2-thienyl)pyrazine 1-oxide

Base Information

Chemical Name:3-methyl-5-[2-({[4-(methyloxy)phenyl]methyl}oxy)phenyl]-2-(5-methyl-2-thienyl)pyrazine 1-oxide
CAS No.:1098194-55-8
Molecular Formula:C₂₄H₂₂N₂O₃S
Molecular Weight:418.516
Hs Code.:

Synonyms:3-methyl-5-[2-({[4-(methyloxy)phenyl]methyl}oxy)phenyl]-2-(5-methyl-2-thienyl)pyrazine 1-oxide

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Chemical Property of 3-methyl-5-[2-({[4-(methyloxy)phenyl]methyl}oxy)phenyl]-2-(5-methyl-2-thienyl)pyrazine 1-oxide

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Technology Process of 3-methyl-5-[2-({[4-(methyloxy)phenyl]methyl}oxy)phenyl]-2-(5-methyl-2-thienyl)pyrazine 1-oxide

There total 1 articles about 3-methyl-5-[2-({[4-(methyloxy)phenyl]methyl}oxy)phenyl]-2-(5-methyl-2-thienyl)pyrazine 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 765-58-2
2-bromo-5-methyl thiophene

: 1098194-54-7
C₁₉H₁₈N₂O₃

: 1098194-55-8
3-methyl-5-[2-({[4-(methyloxy)phenyl]methyl}oxy)phenyl]-2-(5-methyl-2-thienyl)pyrazine 1-oxide

Guidance literature:: With P(t-Bu)2Me*HBF₄; palladium diacetate; potassium carbonate; In toluene; at 110 ℃; for 16h; regioselective reaction;
DOI:10.1016/j.tetlet.2009.12.053

Reference yield: 62.0%

: 3277-89-2
phenethylmagnesium bromide

: 1098194-55-8
3-methyl-5-[2-({[4-(methyloxy)phenyl]methyl}oxy)phenyl]-2-(5-methyl-2-thienyl)pyrazine 1-oxide

: 1213782-95-6
C₃₂H₃₀N₂O₂S

: 1098194-56-9
C₃₂H₃₀N₂O₃S

Guidance literature:: phenethylmagnesium bromide; 3-methyl-5-[2-({[4-(methyloxy)phenyl]methyl}oxy)phenyl]-2-(5-methyl-2-thienyl)pyrazine 1-oxide; In tetrahydrofuran; at -30 ℃;

With oxygen; In tetrahydrofuran; for 1h;
DOI:10.1016/j.tetlet.2009.12.053