Technology Process of 2-allyloxy-4-benzyloxy-5-bromophenol
There total 6 articles about 2-allyloxy-4-benzyloxy-5-bromophenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide; silica gel;
In
dichloromethane;
at 20 ℃;
regioselective reaction;
DOI:10.1021/ol302011b
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / acetone / 6 h / Reflux
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 6 h / Reflux
3: water; potassium carbonate / methanol; ethyl acetate
4: N-Bromosuccinimide; silica gel / dichloromethane / 20 °C
With
N-Bromosuccinimide; water; silica gel; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; ethyl acetate; acetone;
2: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1021/ol302011b
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / acetone / Reflux
2: potassium carbonate / acetone / 6 h / Reflux
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 6 h / Reflux
4: water; potassium carbonate / methanol; ethyl acetate
5: N-Bromosuccinimide; silica gel / dichloromethane / 20 °C
With
N-Bromosuccinimide; water; silica gel; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; ethyl acetate; acetone;
3: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1021/ol302011b
