N-allyl-N-chloro-[2-(3-ethylcyclohex-2-enyl)ethyl]amine

Base Information

Chemical Name:N-allyl-N-chloro-[2-(3-ethylcyclohex-2-enyl)ethyl]amine
CAS No.:880645-25-0
Molecular Formula:C₁₃H₂₂ClN
Molecular Weight:227.777
Hs Code.:

Synonyms:N-allyl-N-chloro-[2-(3-ethylcyclohex-2-enyl)ethyl]amine

Suppliers and Price of N-allyl-N-chloro-[2-(3-ethylcyclohex-2-enyl)ethyl]amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-allyl-N-chloro-[2-(3-ethylcyclohex-2-enyl)ethyl]amine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of N-allyl-N-chloro-[2-(3-ethylcyclohex-2-enyl)ethyl]amine

There total 7 articles about N-allyl-N-chloro-[2-(3-ethylcyclohex-2-enyl)ethyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 880645-33-0
N-allyl-[2-(3-ethylcyclohex-2-enyl)ethyl]amine

: 880645-25-0
N-allyl-N-chloro-[2-(3-ethylcyclohex-2-enyl)ethyl]amine

Guidance literature:: With N-chloro-succinimide; In dichloromethane; at -30 - 18 ℃; for 2h;
DOI:10.3987/COM-05-10575

Reference yield:

: 17299-34-2
3-ethylcyclohex-2-en-1-one

: 880645-25-0
N-allyl-N-chloro-[2-(3-ethylcyclohex-2-enyl)ethyl]amine

Guidance literature:: Multi-step reaction with 7 steps

1.1: 96 percent / sodium borohydride / methanol / 16 h / 18 °C

2.1: 100 percent / DMAP / pyridine / 10 h / 18 °C

3.1: 90 percent / 1,2-bis(diphenylphosphino)ethane; sodium hydride / Pd₂dba3 / tetrahydrofuran / 24 h / Heating

4.1: 80 percent / LiI*3H₂O / dimethylsulfoxide / 1.5 h / 180 °C

5.1: 75 percent / DIBAL-H / CH₂Cl₂; hexane / 1 h / -78 °C

6.1: 4 Angstroem molecular sieves / tetrahydrofuran / 4 h / 18 °C

6.2: 75 percent / sodium borohydride / methanol / 0.3 h / 0 °C

7.1: 97 percent / N-chlorosuccinimide / CH₂Cl₂ / 2 h / -30 - 18 °C

With dmap; sodium tetrahydroborate; N-chloro-succinimide; 4 A molecular sieve; sodium hydride; diisobutylaluminium hydride; 1,2-bis-(diphenylphosphino)ethane; lithium iodide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; dimethyl sulfoxide;
DOI:10.3987/COM-05-10575

Reference yield:

: 5323-87-5
3-Ethoxycyclohex-2-en-1-one

: 880645-25-0
N-allyl-N-chloro-[2-(3-ethylcyclohex-2-enyl)ethyl]amine

Guidance literature:: Multi-step reaction with 8 steps

1.1: 89 percent / diethyl ether; tetrahydrofuran / 3 h / 0 °C

2.1: 96 percent / sodium borohydride / methanol / 16 h / 18 °C

3.1: 100 percent / DMAP / pyridine / 10 h / 18 °C

4.1: 90 percent / 1,2-bis(diphenylphosphino)ethane; sodium hydride / Pd₂dba3 / tetrahydrofuran / 24 h / Heating

5.1: 80 percent / LiI*3H₂O / dimethylsulfoxide / 1.5 h / 180 °C

6.1: 75 percent / DIBAL-H / CH₂Cl₂; hexane / 1 h / -78 °C

7.1: 4 Angstroem molecular sieves / tetrahydrofuran / 4 h / 18 °C

7.2: 75 percent / sodium borohydride / methanol / 0.3 h / 0 °C

8.1: 97 percent / N-chlorosuccinimide / CH₂Cl₂ / 2 h / -30 - 18 °C

With dmap; sodium tetrahydroborate; N-chloro-succinimide; 4 A molecular sieve; sodium hydride; diisobutylaluminium hydride; 1,2-bis-(diphenylphosphino)ethane; lithium iodide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; pyridine; methanol; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide;
DOI:10.3987/COM-05-10575