C₃₈H₅₀O₈Si

Base Information

Chemical Name:C₃₈H₅₀O₈Si
CAS No.:881651-44-1
Molecular Formula:C₃₈H₅₀O₈Si
Molecular Weight:662.896
Hs Code.:

C<sub>38</sub>H<sub>50</sub>O<sub>8</sub>Si

Synonyms:C₃₈H₅₀O₈Si

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Chemical Property of C₃₈H₅₀O₈Si

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Technology Process of C₃₈H₅₀O₈Si

There total 9 articles about C₃₈H₅₀O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 781668-64-2
C₃₈H₄₈O₈Si

: 881651-44-1
C₃₈H₅₀O₈Si

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride; In methanol; at -55 ℃; for 1h;
DOI:10.1021/ja054750q

Reference yield:

: 781668-62-0
C₃₈H₅₀O₈Si

: 881651-44-1
C₃₈H₅₀O₈Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: KHMDS / tetrahydrofuran / 1 h / -78 °C

1.2: tetrahydrofuran / 0.5 h / -78 °C

2.1: 167 mg / Pd(OAc)2 / dimethylsulfoxide / 72 h

3.1: 85 percent / NaBH₄; CeCl₃*7H₂O / methanol / 1 h / -55 °C

With palladium diacetate; sodium tetrahydroborate; cerium(III) chloride; potassium hexamethylsilazane; In tetrahydrofuran; methanol; dimethyl sulfoxide;
DOI:10.1021/ja054750q

Reference yield:

: 781668-58-4
C₄₁H₆₂O₇Si₂

: 881651-44-1
C₃₈H₅₀O₈Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 4-DMAP; pyridine / CH₂Cl₂ / 3 h / 0 °C

2.1: LDA; HMPA; TBSCl / tetrahydrofuran / 72 h / -78 - 25 °C

3.1: 180 mg / DCC; 4-DMAP / CH₂Cl₂ / 2 h / 0 - 25 °C

4.1: 85 percent / HF*pyridine; pyridine / tetrahydrofuran / 5 h / 0 °C

5.1: 90 percent / DMSO; oxalyl chloride; Et₃N / CH₂Cl₂ / -78 - 0 °C

6.1: KHMDS / tetrahydrofuran / 1 h / -78 °C

6.2: tetrahydrofuran / 0.5 h / -78 °C

7.1: 167 mg / Pd(OAc)2 / dimethylsulfoxide / 72 h

8.1: 85 percent / NaBH₄; CeCl₃*7H₂O / methanol / 1 h / -55 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; palladium diacetate; sodium tetrahydroborate; cerium(III) chloride; oxalyl dichloride; potassium hexamethylsilazane; pyridine hydrogenfluoride; tert-butyldimethylsilyl chloride; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; 2.1: Ireland-Claisen rearrangement / 5.1: Swern oxidation;
DOI:10.1021/ja054750q