4,6-bis{2-[(4-allyloxyphenylimino)methyl]-6-tert-butyl-4-methoxy phenoxy}titanium(IV) dichloride

Base Information

Chemical Name:4,6-bis{2-[(4-allyloxyphenylimino)methyl]-6-tert-butyl-4-methoxy phenoxy}titanium(IV) dichloride
CAS No.:1394003-49-6
Molecular Formula:C₄₂H₄₈Cl₂N₂O₆Ti
Molecular Weight:795.639
Hs Code.:

Synonyms:4,6-bis{2-[(4-allyloxyphenylimino)methyl]-6-tert-butyl-4-methoxy phenoxy}titanium(IV) dichloride

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Chemical Property of 4,6-bis{2-[(4-allyloxyphenylimino)methyl]-6-tert-butyl-4-methoxy phenoxy}titanium(IV) dichloride

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Technology Process of 4,6-bis{2-[(4-allyloxyphenylimino)methyl]-6-tert-butyl-4-methoxy phenoxy}titanium(IV) dichloride

There total 4 articles about 4,6-bis{2-[(4-allyloxyphenylimino)methyl]-6-tert-butyl-4-methoxy phenoxy}titanium(IV) dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 762-99-2
titanium(IV) dichlorodiisopropylate

: 1400812-12-5
2-{N-[4-(allyloxy)phenyl]iminomethyl}-6-tert-butyl-4-methoxyphenol

: 1394003-49-6
4,6-bis{2-[(4-allyloxyphenylimino)methyl]-6-tert-butyl-4-methoxy phenoxy}titanium(IV) dichloride

Guidance literature:: In dichloromethane; toluene; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1134/S1070428014110050

Reference yield:

: 88271-75-4
4-(allyloxy)aniline hydrochloride

: 1394003-49-6
4,6-bis{2-[(4-allyloxyphenylimino)methyl]-6-tert-butyl-4-methoxy phenoxy}titanium(IV) dichloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / methanol / Heating

2: dichloromethane; toluene / 24 h / 20 °C / Inert atmosphere

With triethylamine; In methanol; dichloromethane; toluene;
DOI:10.1134/S1070428012080076

Reference yield:

: 1688-69-3
p-allyloxyaniline

: 1394003-49-6
4,6-bis{2-[(4-allyloxyphenylimino)methyl]-6-tert-butyl-4-methoxy phenoxy}titanium(IV) dichloride

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / water; methanol

2: triethylamine / methanol / Heating

3: dichloromethane; toluene / 24 h / 20 °C / Inert atmosphere

With hydrogenchloride; triethylamine; In methanol; dichloromethane; water; toluene;
DOI:10.1134/S1070428012080076