N-{(2S,3S)-2-(furan-2-yl)-3-[2-(methylsulfinyl) phenyl]-4-benzylbutan-2-yl}(S)-p-tolylsulfinamide

Base Information

Chemical Name:N-{(2S,3S)-2-(furan-2-yl)-3-[2-(methylsulfinyl) phenyl]-4-benzylbutan-2-yl}(S)-p-tolylsulfinamide
CAS No.:1333475-73-2
Molecular Formula:C₃₄H₃₃NO₃S₂
Molecular Weight:567.773
Hs Code.:

Synonyms:N-{(2S,3S)-2-(furan-2-yl)-3-[2-(methylsulfinyl) phenyl]-4-benzylbutan-2-yl}(S)-p-tolylsulfinamide

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Chemical Property of N-{(2S,3S)-2-(furan-2-yl)-3-[2-(methylsulfinyl) phenyl]-4-benzylbutan-2-yl}(S)-p-tolylsulfinamide

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Technology Process of N-{(2S,3S)-2-(furan-2-yl)-3-[2-(methylsulfinyl) phenyl]-4-benzylbutan-2-yl}(S)-p-tolylsulfinamide

There total 3 articles about N-{(2S,3S)-2-(furan-2-yl)-3-[2-(methylsulfinyl) phenyl]-4-benzylbutan-2-yl}(S)-p-tolylsulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1333475-66-3
C₁₃H₁₃NO₂S

: C₂₀H₁₈OS

: 1333475-73-2
N-{(2S,3S)-2-(furan-2-yl)-3-[2-(methylsulfinyl) phenyl]-4-benzylbutan-2-yl}(S)-p-tolylsulfinamide

Guidance literature:: C₂₀H₁₈OS; With n-butyllithium; diisopropylamine; In tetrahydrofuran; at -78 - 0 ℃; for 0.166667h; Inert atmosphere;

C₁₃H₁₃NO₂S; In tetrahydrofuran; at -78 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1007/s00726-011-0881-7

Reference yield:

: 1192-62-7,80145-44-4
1-(2-furyl)-1-ethanone

: 1333475-73-2
N-{(2S,3S)-2-(furan-2-yl)-3-[2-(methylsulfinyl) phenyl]-4-benzylbutan-2-yl}(S)-p-tolylsulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium(IV) tetraethanolate / dichloromethane / Heating

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran / 0.17 h / -78 - 0 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

With titanium(IV) tetraethanolate; n-butyllithium; diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1007/s00726-011-0881-7

Reference yield:

: 188447-91-8
(S)-p-toluenesulfinimide

: 1333475-73-2
N-{(2S,3S)-2-(furan-2-yl)-3-[2-(methylsulfinyl) phenyl]-4-benzylbutan-2-yl}(S)-p-tolylsulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium(IV) tetraethanolate / dichloromethane / Heating

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran / 0.17 h / -78 - 0 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

With titanium(IV) tetraethanolate; n-butyllithium; diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1007/s00726-011-0881-7