(E)-1-<4-(methylsulfinyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

Base Information

Chemical Name:(E)-1-<4-(methylsulfinyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene
CAS No.:121887-51-2
Molecular Formula:C₃₀H₂₁F₇O₂S
Molecular Weight:578.55
Hs Code.:

Synonyms:(E)-1-<4-(methylsulfinyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

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Chemical Property of (E)-1-<4-(methylsulfinyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

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Technology Process of (E)-1-<4-(methylsulfinyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

There total 6 articles about (E)-1-<4-(methylsulfinyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 121887-49-8
(E)-1-<4-(methylthio)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

: 121887-51-2
(E)-1-<4-(methylsulfinyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

Guidance literature:: With dihydrogen peroxide; acetic acid; for 2h; Heating;
DOI:10.1021/jm00132a006

Reference yield:

: 104-95-0
(4-bromophenyl)thioanisole

: 121887-51-2
(E)-1-<4-(methylsulfinyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

Guidance literature:: Multi-step reaction with 5 steps

1: 1) Mg, Br(CH₂)2Br / 1) Et₂O, reflux, 2) Et₂O, reflux, 12 h

2: conc. H₂SO₄ / ethanol / 1 h / Ambient temperature

3: 73 percent / pyridine hydrochloride / 2 h / 200 °C

4: 4N>HSO₄, 1 M NaOH / CH₂Cl₂ / 1 h / Ambient temperature

5: 51 percent / H₂O₂, AcOH / 2 h / Heating

With sodium hydroxide; sulfuric acid; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate; pyridine hydrochloride; magnesium; acetic acid; ethylene dibromide; In ethanol; dichloromethane;
DOI:10.1021/jm00132a006

Reference yield:

: 78423-10-6
1-(4-methoxyphenyl)-2-phenylbutan-1-one

: 121887-51-2
(E)-1-<4-(methylsulfinyl)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenylbut-1-ene

Guidance literature:: Multi-step reaction with 5 steps

1: 1) Mg, Br(CH₂)2Br / 1) Et₂O, reflux, 2) Et₂O, reflux, 12 h

2: conc. H₂SO₄ / ethanol / 1 h / Ambient temperature

3: 73 percent / pyridine hydrochloride / 2 h / 200 °C

4: 4N>HSO₄, 1 M NaOH / CH₂Cl₂ / 1 h / Ambient temperature

5: 51 percent / H₂O₂, AcOH / 2 h / Heating

With sodium hydroxide; sulfuric acid; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate; pyridine hydrochloride; magnesium; acetic acid; ethylene dibromide; In ethanol; dichloromethane;
DOI:10.1021/jm00132a006