[4-(hydroxyl)phenyl]phenylpyren-1-ylphosphine borane

Base Information

• Chemical Name: [4-(hydroxyl)phenyl]phenylpyren-1-ylphosphine borane
• CAS No.: 1187472-64-5
• Molecular Formula: C₂₈H₂₂BOP
• Molecular Weight: 416.267
• Mol file: 1187472-64-5.mol

Synonyms:[4-(hydroxyl)phenyl]phenylpyren-1-ylphosphine borane

Chemical Property of [4-(hydroxyl)phenyl]phenylpyren-1-ylphosphine borane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [4-(hydroxyl)phenyl]phenylpyren-1-ylphosphine borane

There total 1 articles about [4-(hydroxyl)phenyl]phenylpyren-1-ylphosphine borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C28H19OP → [4-(hydroxyl)phenyl]phenylpyren-1-ylphosphine borane (1187472-64-5)

Guidance literature:

With borane-THF; In toluene; for 0.25h;

DOI:10.1016/j.bmcl.2010.05.017

Reference yield: 33.0%

[4-(hydroxyl)phenyl]phenylpyren-1-ylphosphine borane (1187472-64-5) + (3-iodopropyl)triphenylphosphonium iodide → [pyrenylphenyl-4-phenoxyphosphineborane]triphenylphosphonium dide (1187472-65-6)

Guidance literature:

[4-(hydroxyl)phenyl]phenylpyren-1-ylphosphine borane; With sodium hydride; In N,N-dimethyl-formamide; for 3h;

(3-iodopropyl)triphenylphosphonium iodide; In N,N-dimethyl-formamide; at -15 - 20 ℃;

DOI:10.1016/j.bmcl.2010.05.017

Downstream raw materials:

[pyrenylphenyl-4-phenoxyphosphineborane]triphenylphosphonium dide