C₂₂H₂₇NO₄

Base Information

Chemical Name:C₂₂H₂₇NO₄
CAS No.:1453083-13-0
Molecular Formula:C₂₂H₂₇NO₄
Molecular Weight:369.461
Hs Code.:

C<sub>22</sub>H<sub>27</sub>NO<sub>4</sub>

Synonyms:C₂₂H₂₇NO₄

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Chemical Property of C₂₂H₂₇NO₄

Chemical Property:

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Technology Process of C₂₂H₂₇NO₄

There total 3 articles about C₂₂H₂₇NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1453083-14-1
(S)-benzyl 4-methoxybenzyl(1-oxopropan-2-yl)carbamate

: 106-95-6
allyl bromide

: 1453083-12-9
C₂₂H₂₇NO₄

: 1453083-13-0
C₂₂H₂₇NO₄

Guidance literature:: With water; ammonium chloride; zinc; In tetrahydrofuran; at 25 - 30 ℃; for 1h; Overall yield = 97 %; Overall yield = 3.5 g;

Reference yield:

: 1453083-15-2
(S)-benzyl (1-hydroxypropan-2-yl)(4-methoxybenzyl)carbamate

: 1453083-13-0
C₂₂H₂₇NO₄

Guidance literature:: Multi-step reaction with 2 steps

1: potassium bromide; sodium hypochlorite; sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 1.5 h / 0 - 5 °C

2: ammonium chloride; water; zinc / tetrahydrofuran / 1 h / 25 - 30 °C

With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water; sodium hydrogencarbonate; ammonium chloride; potassium bromide; zinc; In tetrahydrofuran; dichloromethane; water;

Reference yield:

: 439589-23-8
(S)-2-(((benzyloxy)carbonyl)(4-methoxybenzyl)amino)propanoic acid

: 1453083-13-0
C₂₂H₂₇NO₄

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 0 - 45 °C / Inert atmosphere

2: potassium bromide; sodium hypochlorite; sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 1.5 h / 0 - 5 °C

3: ammonium chloride; water; zinc / tetrahydrofuran / 1 h / 25 - 30 °C

With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; dimethylsulfide borane complex; water; sodium hydrogencarbonate; ammonium chloride; potassium bromide; zinc; In tetrahydrofuran; dichloromethane; water;