1-Benzyldisulfanyl-2-(prop-2-ene-1-sulfinylmethyl)-benzene

Base Information

Chemical Name:1-Benzyldisulfanyl-2-(prop-2-ene-1-sulfinylmethyl)-benzene
CAS No.:106880-24-4
Molecular Formula:C₁₇H₁₈OS₃
Molecular Weight:334.527
Hs Code.:

Synonyms:1-Benzyldisulfanyl-2-(prop-2-ene-1-sulfinylmethyl)-benzene

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Chemical Property of 1-Benzyldisulfanyl-2-(prop-2-ene-1-sulfinylmethyl)-benzene

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Technology Process of 1-Benzyldisulfanyl-2-(prop-2-ene-1-sulfinylmethyl)-benzene

There total 7 articles about 1-Benzyldisulfanyl-2-(prop-2-ene-1-sulfinylmethyl)-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 106880-23-3
1-Allylsulfanylmethyl-2-benzyldisulfanyl-benzene

: 106880-24-4
1-Benzyldisulfanyl-2-(prop-2-ene-1-sulfinylmethyl)-benzene

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 0.166667h; Ambient temperature;
DOI:10.1021/ja00282a033

Reference yield:

: 147-93-3
Thiosalicylic acid

: 106880-24-4
1-Benzyldisulfanyl-2-(prop-2-ene-1-sulfinylmethyl)-benzene

Guidance literature:: Multi-step reaction with 7 steps

1: 90 percent / triethylamine / tetrahydrofuran / 2.5 h / Ambient temperature

2: 93 percent / lithium aluminum hydride / diethyl ether / 8 h / Ambient temperature

3: 91 percent / triethylamine / CH₂Cl₂ / 0.17 h / -10 °C

4: 87 percent / tetrahydrofuran / 0.5 h / Ambient temperature

5: 1.) silver nitrate; 2.) hydrogen sulfide / 1.) water, methanol, heating, 10 min; 2.) methylene chloride, 5 min

6: 96 percent / 1.) n-butyllithium / hexane; tetrahydrofuran / 0.5 h / Ambient temperature

7: 96 percent / 1.) 80 percent MCPBA; 2.) 5 percent sodium bicarbonate / CH₂Cl₂ / 0.17 h / Ambient temperature

With lithium aluminium tetrahydride; n-butyllithium; hydrogen sulfide; sodium hydrogencarbonate; silver nitrate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja00282a033

Reference yield:

: 104324-48-3
allyl (o-mercaptophenyl)methyl sulfide

: 106880-24-4
1-Benzyldisulfanyl-2-(prop-2-ene-1-sulfinylmethyl)-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 1.) n-butyllithium / hexane; tetrahydrofuran / 0.5 h / Ambient temperature

2: 96 percent / 1.) 80 percent MCPBA; 2.) 5 percent sodium bicarbonate / CH₂Cl₂ / 0.17 h / Ambient temperature

With n-butyllithium; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja00282a033