C₃₉H₃₃N₉O₉S

Base Information

Chemical Name:C₃₉H₃₃N₉O₉S
CAS No.:1532530-42-9
Molecular Formula:C₃₉H₃₃N₉O₉S
Molecular Weight:803.812
Hs Code.:

C<sub>39</sub>H<sub>33</sub>N<sub>9</sub>O<sub>9</sub>S

Synonyms:C₃₉H₃₃N₉O₉S

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Chemical Property of C₃₉H₃₃N₉O₉S

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Technology Process of C₃₉H₃₃N₉O₉S

There total 6 articles about C₃₉H₃₃N₉O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1532530-36-1
C₂₉H₂₁BrN₈O₈S

: 186498-02-2
4-(4-morpholinyl)phenylboronic acid

: 1532530-42-9
C₃₉H₃₃N₉O₉S

Guidance literature:: With potassium fluoride; palladium diacetate; at 80 ℃; for 24h; Inert atmosphere;
DOI:10.1246/bcsj.20130198

Reference yield:

: 1532530-28-1
C₂₉H₂₅BrN₈O₉S

: 1532530-42-9
C₃₉H₃₃N₉O₉S

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; methanesulfonyl chloride / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C / Inert atmosphere

2.1: N-Bromosuccinimide / methanol; dichloromethane / 2 h / 0 °C / Molecular sieve; Inert atmosphere

2.2: 8 h / 60 °C / Inert atmosphere

2.3: 14 h / 70 °C / Molecular sieve; Inert atmosphere

3.1: palladium diacetate; potassium fluoride / 24 h / 80 °C / Inert atmosphere

With potassium fluoride; N-Bromosuccinimide; palladium diacetate; methanesulfonyl chloride; triethylamine; In methanol; dichloromethane; 3.1: |Suzuki-Miyaura Coupling;
DOI:10.1246/bcsj.20130198

Reference yield:

: 912656-51-0
2''',2'''-dimethyl-4''',5'''-dihydro-[2,4';2',4'';2'',4''']quateroxazole-4,3'''-dicarboxylic acid 4-benzyl ester 3'''-tert-butyl ester

: 1532530-42-9
C₃₉H₃₃N₉O₉S

Guidance literature:: Multi-step reaction with 5 steps

1.1: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 2 h / 20 °C / Inert atmosphere

1.2: 6 h / 0 - 20 °C

1.3: 3 h / 0 - 20 °C / Inert atmosphere

2.1: trimethyltin(IV) hydroxide / 1,2-dichloro-ethane / 8 h / 80 °C / Inert atmosphere

2.2: 4 h / 0 - 20 °C

2.3: 72 h / 20 °C / Inert atmosphere

3.1: triethylamine; methanesulfonyl chloride / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

3.2: 2 h / 0 - 20 °C / Inert atmosphere

4.1: N-Bromosuccinimide / methanol; dichloromethane / 2 h / 0 °C / Molecular sieve; Inert atmosphere

4.2: 8 h / 60 °C / Inert atmosphere

4.3: 14 h / 70 °C / Molecular sieve; Inert atmosphere

5.1: palladium diacetate; potassium fluoride / 24 h / 80 °C / Inert atmosphere

With potassium fluoride; N-Bromosuccinimide; palladium 10% on activated carbon; hydrogen; palladium diacetate; methanesulfonyl chloride; triethylamine; trimethyltin(IV) hydroxide; In methanol; dichloromethane; ethyl acetate; 1,2-dichloro-ethane; 5.1: |Suzuki-Miyaura Coupling;
DOI:10.1246/bcsj.20130198