2-(trimethylsilyl)ethyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→4)-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→4)-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:1441126-81-3
Molecular Formula:C₇₉H₈₈O₁₇Si
Molecular Weight:1337.64
Hs Code.:

2-(trimethylsilyl)ethyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→4)-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Synonyms:2-(trimethylsilyl)ethyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→4)-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of 2-(trimethylsilyl)ethyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→4)-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of 2-(trimethylsilyl)ethyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→4)-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 1 articles about 2-(trimethylsilyl)ethyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→4)-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1441126-77-7
2-(trimethylsilyl)ethyl (2-O-benzyl-4,6-O-benzylidene-3-O-chloroacetyl-α-D-galactopyranosyl)-(1→4)-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1441126-81-3
2-(trimethylsilyl)ethyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→4)-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With 2,6-dimethylpyridine; thiourea; In N,N-dimethyl-formamide; at 20 - 50 ℃; for 14h;
DOI:10.1002/chem.201203865

Reference yield: 92.0%

: 1441126-81-3
2-(trimethylsilyl)ethyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→4)-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1441126-85-7
2,6-dimethylphenyl (2-azido-4,6-O-benzylidene-3-O-chloroacetyl-2-deoxy-α-D-galactopyranosyl)-(1→3)-1-thio-4,6-O-benzylidene-2-deoxy-2-(2,2,2,-trichloroethoxycarbonylamino)-β-D-galactopyranoside

: 1441126-89-1
2-(trimethylsilyl)ethyl (2-azido-4,6-O-benzylidene-3-O-chloroacetyl-2-deoxy-α-D-galactopyranosyl)-(1→3)-[4,6-O-benzylidene-2-deoxy-2-(2,2,2,-trichloroethoxycarbonylamino)-β-D-galactopyranosyl]-(1→3)-(2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→4)-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -20 - 0 ℃; for 2h; Inert atmosphere; Molecular sieve;
DOI:10.1002/chem.201203865

Reference yield:

: 1441126-81-3
2-(trimethylsilyl)ethyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→4)-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: C₄₆H₄₇Cl₄NO₁₂S

: 1441126-99-3
2-(trimethylsilyl)ethyl (2-O-benzyl-4,6-O-benzylidene-3-O-chloroacetyl-α-D-galactopyranosyl)-(1→3)-[4,6-O-benzylidene-2-deoxy-2-(2,2,2,-trichloroethoxycarbonylamino)-β-D-galactopyranosyl]-(1→3)-(2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1→4)-(2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; In dichloromethane; at -25 ℃; for 2h; Inert atmosphere; Molecular sieve;
DOI:10.1002/chem.201203865