1-(2-chloro-6-methylphenyl)-(1,2-dideoxy-α-D-glucofurano)[2,1-d]imidazolidine-2-thione

Base Information

• Chemical Name: 1-(2-chloro-6-methylphenyl)-(1,2-dideoxy-α-D-glucofurano)[2,1-d]imidazolidine-2-thione
• CAS No.: 258879-37-7
• Molecular Formula: C₁₄H₁₇ClN₂O₄S
• Molecular Weight: 344.819

Synonyms:1-(2-chloro-6-methylphenyl)-(1,2-dideoxy-α-D-glucofurano)[2,1-d]imidazolidine-2-thione

Chemical Property of 1-(2-chloro-6-methylphenyl)-(1,2-dideoxy-α-D-glucofurano)[2,1-d]imidazolidine-2-thione

Chemical Property:

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Technology Process of 1-(2-chloro-6-methylphenyl)-(1,2-dideoxy-α-D-glucofurano)[2,1-d]imidazolidine-2-thione

There total 4 articles about 1-(2-chloro-6-methylphenyl)-(1,2-dideoxy-α-D-glucofurano)[2,1-d]imidazolidine-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3R,4R,5S,6R)-6-(acetoxymethyl)-3-aminotetrahydro-2H-pyran-2,4,5-triyl triacetate (59042-16-9) → 1-(2-chloro-6-methylphenyl)-(1,2-dideoxy-α-D-glucofurano)[2,1-d]imidazolidine-2-thione (258879-37-7)

Guidance literature:

Multi-step reaction with 3 steps

1: CH₂Cl₂ / 72 h / 20 °C

2: NH₃; MeOH

3: 30 percent AcOH / 0.5 h / Heating

With methanol; ammonia; acetic acid; In dichloromethane;

DOI:10.1016/S0957-4166(99)00428-0

Reference yield:

2-chloro-6-methylphenyl isothiocyanate (19241-34-0) → 1-(2-chloro-6-methylphenyl)-(1,2-dideoxy-α-D-glucofurano)[2,1-d]imidazolidine-2-thione (258879-37-7)

Guidance literature:

Multi-step reaction with 3 steps

1: CH₂Cl₂ / 72 h / 20 °C

2: NH₃; MeOH

3: 30 percent AcOH / 0.5 h / Heating

With methanol; ammonia; acetic acid; In dichloromethane;

DOI:10.1016/S0957-4166(99)00428-0

Reference yield:

1-(2-Chloro-6-methyl-phenyl)-3-((3R,4R,5S,6R)-2,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-thiourea → 1-(2-chloro-6-methylphenyl)-(1,2-dideoxy-α-D-glucofurano)[2,1-d]imidazolidine-2-thione (258879-37-7)

Guidance literature:

With acetic acid; for 0.5h; Heating;

DOI:10.1016/S0957-4166(99)00428-0

upstream raw materials:

(3R,4R,5S,6R)-6-(acetoxymethyl)-3-aminotetrahydro-2H-pyran-2,4,5-triyl triacetate

2-chloro-6-methylphenyl isothiocyanate

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