3-[benzyl-(4-methoxy-benzenesulfonyl)-amino]-2,6-dimethoxy-isonicotinic acid

Base Information

Chemical Name:3-[benzyl-(4-methoxy-benzenesulfonyl)-amino]-2,6-dimethoxy-isonicotinic acid
CAS No.:206192-72-5
Molecular Formula:C₂₂H₂₂N₂O₇S
Molecular Weight:458.492
Hs Code.:

Synonyms:3-[benzyl-(4-methoxy-benzenesulfonyl)-amino]-2,6-dimethoxy-isonicotinic acid

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Chemical Property of 3-[benzyl-(4-methoxy-benzenesulfonyl)-amino]-2,6-dimethoxy-isonicotinic acid

Chemical Property:

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Technology Process of 3-[benzyl-(4-methoxy-benzenesulfonyl)-amino]-2,6-dimethoxy-isonicotinic acid

There total 7 articles about 3-[benzyl-(4-methoxy-benzenesulfonyl)-amino]-2,6-dimethoxy-isonicotinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 206192-71-4
methyl 3-[Benzyl-(4-methoxy-benzenesulfonyl)-amino]-2,6-dimethoxy-isonicotinate

: 206192-72-5
3-[benzyl-(4-methoxy-benzenesulfonyl)-amino]-2,6-dimethoxy-isonicotinic acid

Guidance literature:: With lithium hydroxide;
DOI:10.1016/S0960-894X(00)00644-2

Reference yield:

: 28020-37-3
2,6-dimethoxy-3-aminopyridine

: 206192-72-5
3-[benzyl-(4-methoxy-benzenesulfonyl)-amino]-2,6-dimethoxy-isonicotinic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 34 percent / n-BuLi; TMEDA

2: p-TsOH

3: TEA

4: 100 percent / NaH

5: LiOH

With lithium hydroxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; TEA; sodium hydride; toluene-4-sulfonic acid;
DOI:10.1016/S0960-894X(00)00644-2

Reference yield:

: 161117-86-8
3-(tert-butoxycarbonylamino)-2,6-dimethoxypyridine

: 206192-72-5
3-[benzyl-(4-methoxy-benzenesulfonyl)-amino]-2,6-dimethoxy-isonicotinic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 34 percent / n-BuLi; TMEDA

2: p-TsOH

3: TEA

4: 100 percent / NaH

5: LiOH

With lithium hydroxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; TEA; sodium hydride; toluene-4-sulfonic acid;
DOI:10.1016/S0960-894X(00)00644-2