Phenyl-phosphoramidic acid benzyl ester phenyl ester

Base Information

Chemical Name:Phenyl-phosphoramidic acid benzyl ester phenyl ester
CAS No.:206869-85-4
Molecular Formula:C₁₉H₁₈NO₃P
Molecular Weight:339.331
Hs Code.:

Synonyms:Phenyl-phosphoramidic acid benzyl ester phenyl ester

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Chemical Property of Phenyl-phosphoramidic acid benzyl ester phenyl ester

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Technology Process of Phenyl-phosphoramidic acid benzyl ester phenyl ester

There total 3 articles about Phenyl-phosphoramidic acid benzyl ester phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Phenyl-phosphoramidous acid benzyl ester phenyl ester

: 206869-85-4
Phenyl-phosphoramidic acid benzyl ester phenyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 1h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4020(98)00123-9

Reference yield:

: 76101-29-6
benzyloxy dichlorophosphine

: 206869-85-4
Phenyl-phosphoramidic acid benzyl ester phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) diisopropylethylamine / 1.) ether, -78 deg C, 4 h, 2.) ether, -78 deg C, 3.5 h, then room temp., 1 h

2: m-CPBA / CH₂Cl₂ / 1 h / Ambient temperature

With N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/S0040-4020(98)00123-9

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 206869-85-4
Phenyl-phosphoramidic acid benzyl ester phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / PCl₃ / diethyl ether / 2 h / -40 °C

2: 1.) diisopropylethylamine / 1.) ether, -78 deg C, 4 h, 2.) ether, -78 deg C, 3.5 h, then room temp., 1 h

3: m-CPBA / CH₂Cl₂ / 1 h / Ambient temperature

With N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; phosphorus trichloride; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(98)00123-9