(E)-1-[(p-bromomethyl)phenyl]sulfonyl-2-phenylseleno-2-trimethylsilylethene

Base Information

Chemical Name:(E)-1-[(p-bromomethyl)phenyl]sulfonyl-2-phenylseleno-2-trimethylsilylethene
CAS No.:877931-66-3
Molecular Formula:C₁₈H₂₁BrO₂SSeSi
Molecular Weight:488.379
Hs Code.:

Synonyms:(E)-1-[(p-bromomethyl)phenyl]sulfonyl-2-phenylseleno-2-trimethylsilylethene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-[(p-bromomethyl)phenyl]sulfonyl-2-phenylseleno-2-trimethylsilylethene

Chemical Property:

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Technology Process of (E)-1-[(p-bromomethyl)phenyl]sulfonyl-2-phenylseleno-2-trimethylsilylethene

There total 3 articles about (E)-1-[(p-bromomethyl)phenyl]sulfonyl-2-phenylseleno-2-trimethylsilylethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 877931-62-9
Se-phenyl p-(bromomethyl)benzeneselenosulfonate

: 1066-54-2
trimethylsilylacetylene

: 877931-66-3
(E)-1-[(p-bromomethyl)phenyl]sulfonyl-2-phenylseleno-2-trimethylsilylethene

Guidance literature:: In chloroform; for 1h; Irradiation;
DOI:10.1039/b512016k

Reference yield:

: 66176-39-4
4-(bromomethyl)benzene-1-sulfonyl chloride

: 877931-66-3
(E)-1-[(p-bromomethyl)phenyl]sulfonyl-2-phenylseleno-2-trimethylsilylethene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / hydrazine hydrate / tetrahydrofuran; H₂O / 0.25 h / cooling

2: 90 percent / methanol / -20 °C

3: 93 percent / CHCl₃ / 1 h / Irradiation

With hydrazine hydrate; In tetrahydrofuran; methanol; chloroform; water;
DOI:10.1039/b512016k

Reference yield:

: 877931-61-8
p-(bromomethyl)benzenosulfonylhydrazide

: 877931-66-3
(E)-1-[(p-bromomethyl)phenyl]sulfonyl-2-phenylseleno-2-trimethylsilylethene

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / methanol / -20 °C

2: 93 percent / CHCl₃ / 1 h / Irradiation

In methanol; chloroform;
DOI:10.1039/b512016k