p-(benzoyloxy)-benzyl 6-O-benzyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-3-O-(9-fluorenylmethoxycarbonyl)-4-O-(3,4,6-tri-O-benzyl-2-O-levulinoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:p-(benzoyloxy)-benzyl 6-O-benzyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-3-O-(9-fluorenylmethoxycarbonyl)-4-O-(3,4,6-tri-O-benzyl-2-O-levulinoyl-β-D-galactopyranosyl)-β-D-glucopyranoside
CAS No.:869001-83-2
Molecular Formula:C₇₇H₇₄Cl₃NO₁₈
Molecular Weight:1407.79
Hs Code.:

p-(benzoyloxy)-benzyl 6-O-benzyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-3-O-(9-fluorenylmethoxycarbonyl)-4-O-(3,4,6-tri-O-benzyl-2-O-levulinoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Synonyms:p-(benzoyloxy)-benzyl 6-O-benzyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-3-O-(9-fluorenylmethoxycarbonyl)-4-O-(3,4,6-tri-O-benzyl-2-O-levulinoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Chemical Property of p-(benzoyloxy)-benzyl 6-O-benzyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-3-O-(9-fluorenylmethoxycarbonyl)-4-O-(3,4,6-tri-O-benzyl-2-O-levulinoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Technology Process of p-(benzoyloxy)-benzyl 6-O-benzyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-3-O-(9-fluorenylmethoxycarbonyl)-4-O-(3,4,6-tri-O-benzyl-2-O-levulinoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

There total 3 articles about p-(benzoyloxy)-benzyl 6-O-benzyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-3-O-(9-fluorenylmethoxycarbonyl)-4-O-(3,4,6-tri-O-benzyl-2-O-levulinoyl-β-D-galactopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 869002-02-8
p-(benzoyloxy)-benzyl 6-O-benzyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-3-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranoside

: 4-Oxo-pentanoic acid (2S,3R,4S,5S,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-ethylsulfanyl-tetrahydro-pyran-3-yl ester

: 869001-83-2
p-(benzoyloxy)-benzyl 6-O-benzyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-3-O-(9-fluorenylmethoxycarbonyl)-4-O-(3,4,6-tri-O-benzyl-2-O-levulinoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; 3 A molecular sieve; triethylsilyl trifluoromethyl sulfonate; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1002/chem.200500412

Reference yield:

: 87770-86-3
p-(hydroxymethyl)phenyl benzoate

: 869001-83-2
p-(benzoyloxy)-benzyl 6-O-benzyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-3-O-(9-fluorenylmethoxycarbonyl)-4-O-(3,4,6-tri-O-benzyl-2-O-levulinoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / N-iodosuccinimide; TESOTf; 3 Angstroem molecular sieves / CH₂Cl₂ / 0.5 h / 0 °C

2: 81 percent / N-iodosuccinimide; TESOTf; 3 Angstroem molecular sieves / CH₂Cl₂ / 0.5 h / 0 °C

With N-iodo-succinimide; 3 A molecular sieve; triethylsilyl trifluoromethyl sulfonate; In dichloromethane;
DOI:10.1002/chem.200500412

Reference yield:

: Carbonic acid (2R,3S,4R,5R,6S)-2-benzyloxymethyl-6-ethylsulfanyl-3-hydroxy-5-(2,2,2-trichloro-ethoxycarbonylamino)-tetrahydro-pyran-4-yl ester 9H-fluoren-9-ylmethyl ester

: 869001-83-2
p-(benzoyloxy)-benzyl 6-O-benzyl-2-deoxy-2-[[(2,2,2-trichloroethoxy)carbonyl]amino]-3-O-(9-fluorenylmethoxycarbonyl)-4-O-(3,4,6-tri-O-benzyl-2-O-levulinoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / N-iodosuccinimide; TESOTf; 3 Angstroem molecular sieves / CH₂Cl₂ / 0.5 h / 0 °C

2: 81 percent / N-iodosuccinimide; TESOTf; 3 Angstroem molecular sieves / CH₂Cl₂ / 0.5 h / 0 °C

With N-iodo-succinimide; 3 A molecular sieve; triethylsilyl trifluoromethyl sulfonate; In dichloromethane;
DOI:10.1002/chem.200500412