C₂₉H₄₁ClO₄

Base Information

Chemical Name:C₂₉H₄₁ClO₄
CAS No.:1616095-11-4
Molecular Formula:C₂₉H₄₁ClO₄
Molecular Weight:489.095
Hs Code.:

C<sub>29</sub>H<sub>41</sub>ClO<sub>4</sub>

Synonyms:C₂₉H₄₁ClO₄

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Chemical Property of C₂₉H₄₁ClO₄

Chemical Property:

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Technology Process of C₂₉H₄₁ClO₄

There total 8 articles about C₂₉H₄₁ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616094-96-2
C₂₈H₄₀O₅

: 1616094-97-3
C₂₉H₄₁ClO₄

: 1616095-11-4
C₂₉H₄₁ClO₄

Guidance literature:: With chromium dichloride; chloroform; In tetrahydrofuran; at 65 ℃; for 4h; Overall yield = 65 %; Overall yield = 40 mg; Sealed tube; Inert atmosphere;
DOI:10.1016/j.tet.2014.04.090

Reference yield:

: 1616094-89-3
C₂₆H₃₈O₆

: 1616094-97-3
C₂₉H₄₁ClO₄

: 1616095-11-4
C₂₉H₄₁ClO₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: triphenylphosphine; 1H-imidazole; iodine / tetrahydrofuran / 1 h / 60 - 80 °C

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / diethyl ether / 20 °C / Inert atmosphere

2.2: air / 5 h

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; nickel; hydrogen / methanol / 1 h

4.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 2 h / 20 °C

5.1: chloroform; chromium dichloride / tetrahydrofuran / 4 h / 65 °C / Sealed tube; Inert atmosphere

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; chromium dichloride; chloroform; hydrogen; iodine; nickel; sodium hydrogencarbonate; Dess-Martin periodane; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2014.04.090

Reference yield:

: 1616094-90-6
C₂₆H₃₆O₄

: 1616094-97-3
C₂₉H₄₁ClO₄

: 1616095-11-4
C₂₉H₄₁ClO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / diethyl ether / 20 °C / Inert atmosphere

1.2: air / 5 h

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; nickel; hydrogen / methanol / 1 h

3.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 2 h / 20 °C

4.1: chloroform; chromium dichloride / tetrahydrofuran / 4 h / 65 °C / Sealed tube; Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; chromium dichloride; chloroform; hydrogen; nickel; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2014.04.090