N₁-{[3-bromo-5-(methyloxy)phenyl]methyl}-N₂-{[1,6-diethyl-4-(tetrahydro-2H-pyran-4-ylamino)-1H-pyrazolo[3,4-b]pyridin-5-yl]methyl}-1,3-benzenedicarboxamide

Base Information

• Chemical Name: N₁-{[3-bromo-5-(methyloxy)phenyl]methyl}-N₂-{[1,6-diethyl-4-(tetrahydro-2H-pyran-4-ylamino)-1H-pyrazolo[3,4-b]pyridin-5-yl]methyl}-1,3-benzenedicarboxamide
• CAS No.: 1177559-07-7
• Molecular Formula: C₃₂H₃₇BrN₆O₄
• Molecular Weight: 649.588

Synonyms:N₁-{[3-bromo-5-(methyloxy)phenyl]methyl}-N₂-{[1,6-diethyl-4-(tetrahydro-2H-pyran-4-ylamino)-1H-pyrazolo[3,4-b]pyridin-5-yl]methyl}-1,3-benzenedicarboxamide

Chemical Property of N₁-{[3-bromo-5-(methyloxy)phenyl]methyl}-N₂-{[1,6-diethyl-4-(tetrahydro-2H-pyran-4-ylamino)-1H-pyrazolo[3,4-b]pyridin-5-yl]methyl}-1,3-benzenedicarboxamide

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Technology Process of N₁-{[3-bromo-5-(methyloxy)phenyl]methyl}-N₂-{[1,6-diethyl-4-(tetrahydro-2H-pyran-4-ylamino)-1H-pyrazolo[3,4-b]pyridin-5-yl]methyl}-1,3-benzenedicarboxamide

There total 1 articles about N₁-{[3-bromo-5-(methyloxy)phenyl]methyl}-N₂-{[1,6-diethyl-4-(tetrahydro-2H-pyran-4-ylamino)-1H-pyrazolo[3,4-b]pyridin-5-yl]methyl}-1,3-benzenedicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(3-bromo-5-methoxyphenyl)methanamine (1177558-46-1) + 3-[({[1,6-diethyl-4-(tetrahydro-2H-pyran-4-ylamino)-1H-pyrazolo[3,4-b]pyridin-5-yl]methyl}amino)carbonyl]benzoic acid (1177558-35-8) → N1-{[3-bromo-5-(methyloxy)phenyl]methyl}-N2-{[1,6-diethyl-4-(tetrahydro-2H-pyran-4-ylamino)-1H-pyrazolo[3,4-b]pyridin-5-yl]methyl}-1,3-benzenedicarboxamide (1177559-07-7)

Guidance literature:

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; at 20 ℃;

Reference yield: 85.0%

N1-{[3-bromo-5-(methyloxy)phenyl]methyl}-N2-{[1,6-diethyl-4-(tetrahydro-2H-pyran-4-ylamino)-1H-pyrazolo[3,4-b]pyridin-5-yl]methyl}-1,3-benzenedicarboxamide (1177559-07-7) + 3-Formylphenylboronic acid (87199-16-4) → N-{[1,6-diethyl-4-(tetrahydro-2H-pyran-4-ylamino)-1H-pyrazolo[3,4-b]pyridin-5-yl]methyl}-N'-{[3'-formyl-5-(methyloxy)-3-biphenylyl]methyl}-1,3-benzenedicarboxamide (1177559-08-8)

Guidance literature:

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 150 ℃; for 0.5h; Microwave irradiation;

upstream raw materials:

(3-bromo-5-methoxyphenyl)methanamine

3-[({[1,6-diethyl-4-(tetrahydro-2H-pyran-4-ylamino)-1H-pyrazolo[3,4-b]pyridin-5-yl]methyl}amino)carbonyl]benzoic acid

Downstream raw materials:

N-{[1,6-diethyl-4-(tetrahydro-2H-pyran-4-ylamino)-1H-pyrazolo[3,4-b]pyridin-5-yl]methyl}-N'-{[3'-formyl-5-(methyloxy)-3-biphenylyl]methyl}-1,3-benzenedicarboxamide

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