2-[(toluene-4-sulphonyl)(2-trifluoromethane-sulphonyloxyethyl)amino]ethyl trifluoromethanesulphonate

Base Information

Chemical Name:2-[(toluene-4-sulphonyl)(2-trifluoromethane-sulphonyloxyethyl)amino]ethyl trifluoromethanesulphonate
CAS No.:1271521-53-9
Molecular Formula:C₁₃H₁₅F₆NO₈S₃
Molecular Weight:523.452
Hs Code.:

Synonyms:2-[(toluene-4-sulphonyl)(2-trifluoromethane-sulphonyloxyethyl)amino]ethyl trifluoromethanesulphonate

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Chemical Property of 2-[(toluene-4-sulphonyl)(2-trifluoromethane-sulphonyloxyethyl)amino]ethyl trifluoromethanesulphonate

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Technology Process of 2-[(toluene-4-sulphonyl)(2-trifluoromethane-sulphonyloxyethyl)amino]ethyl trifluoromethanesulphonate

There total 1 articles about 2-[(toluene-4-sulphonyl)(2-trifluoromethane-sulphonyloxyethyl)amino]ethyl trifluoromethanesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 42137-88-2
N,N-bis(2-chloroethyl)-p-toluenesulfonamide

: 1271521-53-9
2-[(toluene-4-sulphonyl)(2-trifluoromethane-sulphonyloxyethyl)amino]ethyl trifluoromethanesulphonate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 18h;

Reference yield: 60.0%

: 1271521-53-9
2-[(toluene-4-sulphonyl)(2-trifluoromethane-sulphonyloxyethyl)amino]ethyl trifluoromethanesulphonate

: methyl (S)-2-amino-3-tert-butoxycarbonylaminopropanoate hydrochloride

: 1271521-54-0
methyl (S)-3-tert-butoxycarbonylamino-2-[4-(toluene-4-sulphonyl)piperazin-1-yl]propanoate

Guidance literature:: With potassium carbonate; In acetonitrile; at 60 ℃; for 18h;

Reference yield:

: 1271521-53-9
2-[(toluene-4-sulphonyl)(2-trifluoromethane-sulphonyloxyethyl)amino]ethyl trifluoromethanesulphonate

: 1271521-56-2
methyl (S)-3-(4-but-2-ynyloxybenzoylamino)-2-[4-(toluene-4-sulphonyl)piperazin-1-yl]propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetonitrile / 18 h / 60 °C

2.1: trifluoroacetic acid / dichloromethane / 18 h / 20 °C

2.2: pH 8

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 17 h / 20 °C

With potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;