Technology Process of 1-(6-Benzyloxy-2-hydroxy-3,4-dimethoxy-phenyl)-decan-1-one
There total 9 articles about 1-(6-Benzyloxy-2-hydroxy-3,4-dimethoxy-phenyl)-decan-1-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: aluminum chloride / diethyl ether / 0.5 h / 0 °C
2: aluminum chloride / acetonitrile / 2 h / 50 °C
3: 83 percent / potassium carbonate / acetone / Heating
4: 90 percent / aluminum bromide / acetonitrile / 3 h / Ambient temperature
5: 83 percent / potassium carbonate / methanol / Heating
6: potassium carbonate / dimethylformamide / 0.33 h / 150 - 160 °C
7: concd. hydrochloric acid, acetic acid / 3 h / Ambient temperature
With
hydrogenchloride; aluminium trichloride; aluminum tri-bromide; potassium carbonate; acetic acid;
In
methanol; diethyl ether; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/jm00111a037
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / dimethylformamide / 0.33 h / 150 - 160 °C
2: concd. hydrochloric acid, acetic acid / 3 h / Ambient temperature
With
hydrogenchloride; potassium carbonate; acetic acid;
In
N,N-dimethyl-formamide;
DOI:10.1021/jm00111a037
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / dimethylformamide / 0.33 h / 150 - 160 °C
2: concd. hydrochloric acid, acetic acid / 3 h / Ambient temperature
With
hydrogenchloride; potassium carbonate; acetic acid;
In
N,N-dimethyl-formamide;
DOI:10.1021/jm00111a037
