2-amino-3'-isopropoxy-4,4',5-trimethoxybenzophenone

Base Information

Chemical Name:2-amino-3'-isopropoxy-4,4',5-trimethoxybenzophenone
CAS No.:212489-70-8
Molecular Formula:C₁₉H₂₃NO₅
Molecular Weight:345.395
Hs Code.:

Synonyms:2-amino-3'-isopropoxy-4,4',5-trimethoxybenzophenone

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Chemical Property of 2-amino-3'-isopropoxy-4,4',5-trimethoxybenzophenone

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Technology Process of 2-amino-3'-isopropoxy-4,4',5-trimethoxybenzophenone

There total 5 articles about 2-amino-3'-isopropoxy-4,4',5-trimethoxybenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 212490-37-4
3-(3-Isopropoxy-4-methoxy-phenyl)-5,6-dimethoxy-1H-indole-2-carboxylic acid methyl ester

: 212489-70-8
2-amino-3'-isopropoxy-4,4',5-trimethoxybenzophenone

Guidance literature:: With chromium(VI) oxide; acetic acid; In water; at 50 ℃; for 4h;
DOI:10.1248/cpb.46.1130

Reference yield:

: 34123-66-5
O-isopropylisovanillin

: 212489-70-8
2-amino-3'-isopropoxy-4,4',5-trimethoxybenzophenone

Guidance literature:: Multi-step reaction with 5 steps

1: piperidine, AcOH / benzene / 6 h / Heating

2: 5percent Pd/C / tetrahydrofuran; ethanol / 760 Torr / Ambient temperature

3: 1.) aq. NaNO₂, aq. HCl, 2.) NaOAc / 1.) acetone, 0-5 deg C, 1 h, 2.) H₂O, acetone, RT, 2 h

4: 54 percent / conc. H₂SO₄ / methanol / 10 h / Heating

5: 50 percent / CrO₃, AcOH / H₂O / 4 h / 50 °C

With piperidine; chromium(VI) oxide; hydrogenchloride; palladium on activated charcoal; sulfuric acid; sodium acetate; acetic acid; sodium nitrite; In tetrahydrofuran; methanol; ethanol; water; benzene;
DOI:10.1248/cpb.46.1130

Reference yield:

: 212490-08-9
2-(3-Isopropoxy-4-methoxy-benzyl)-3-oxo-butyric acid methyl ester

: 212489-70-8
2-amino-3'-isopropoxy-4,4',5-trimethoxybenzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) aq. NaNO₂, aq. HCl, 2.) NaOAc / 1.) acetone, 0-5 deg C, 1 h, 2.) H₂O, acetone, RT, 2 h

2: 54 percent / conc. H₂SO₄ / methanol / 10 h / Heating

3: 50 percent / CrO₃, AcOH / H₂O / 4 h / 50 °C

With chromium(VI) oxide; hydrogenchloride; sulfuric acid; sodium acetate; acetic acid; sodium nitrite; In methanol; water;
DOI:10.1248/cpb.46.1130