(-)-(3R,5S)-methyl 2-benzyl-3-ethyl-5-formyl-5-methylisoxazolidine-3-carboxylate

Base Information

Chemical Name:(-)-(3R,5S)-methyl 2-benzyl-3-ethyl-5-formyl-5-methylisoxazolidine-3-carboxylate
CAS No.:1593585-83-1
Molecular Formula:C₁₆H₂₁NO₄
Molecular Weight:291.347
Hs Code.:

Synonyms:(-)-(3R,5S)-methyl 2-benzyl-3-ethyl-5-formyl-5-methylisoxazolidine-3-carboxylate

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Chemical Property of (-)-(3R,5S)-methyl 2-benzyl-3-ethyl-5-formyl-5-methylisoxazolidine-3-carboxylate

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Technology Process of (-)-(3R,5S)-methyl 2-benzyl-3-ethyl-5-formyl-5-methylisoxazolidine-3-carboxylate

There total 1 articles about (-)-(3R,5S)-methyl 2-benzyl-3-ethyl-5-formyl-5-methylisoxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 78-85-3,25120-30-3
2-methylpropenal

: 1206188-41-1
C₁₂H₁₅NO₃

: 1593585-83-1
(-)-(3R,5S)-methyl 2-benzyl-3-ethyl-5-formyl-5-methylisoxazolidine-3-carboxylate

: (-)-(3S,5R)-methyl 2-benzyl-3-ethyl-5-formyl-5-methylisoxazolidine-3-carboxylate

Guidance literature:: C₁₂H₁₅NO₃; With [Ru(η5-cyclopentadienyl)(BIPHOP-F)(acetone)][SbF6]; In tert-butyl methyl ether; at -10 ℃; for 0.0833333h; Inert atmosphere;

2-methylpropenal; In tert-butyl methyl ether; at -10 ℃; for 168h; Overall yield = 91 %; Overall yield = 66.4 mg; enantioselective reaction; Inert atmosphere;
DOI:10.1021/jo5001737