N-(3β-acetoxy-urs-12-en-28-oyl)-1-amino-N-(2-amino-3-phenyl-1-propionyl-)-2-aminoethane

Base Information

Chemical Name:N-(3β-acetoxy-urs-12-en-28-oyl)-1-amino-N-(2-amino-3-phenyl-1-propionyl-)-2-aminoethane
CAS No.:1351856-48-8
Molecular Formula:C₄₃H₆₅N₃O₄
Molecular Weight:688.007
Hs Code.:

Synonyms:N-(3β-acetoxy-urs-12-en-28-oyl)-1-amino-N-(2-amino-3-phenyl-1-propionyl-)-2-aminoethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3β-acetoxy-urs-12-en-28-oyl)-1-amino-N-(2-amino-3-phenyl-1-propionyl-)-2-aminoethane

Chemical Property:

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Technology Process of N-(3β-acetoxy-urs-12-en-28-oyl)-1-amino-N-(2-amino-3-phenyl-1-propionyl-)-2-aminoethane

There total 4 articles about N-(3β-acetoxy-urs-12-en-28-oyl)-1-amino-N-(2-amino-3-phenyl-1-propionyl-)-2-aminoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.8%

: 1370289-75-0
C₅₈H₇₅N₃O₆

: 1351856-48-8
N-(3β-acetoxy-urs-12-en-28-oyl)-1-amino-N-(2-amino-3-phenyl-1-propionyl-)-2-aminoethane

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2012.02.009

Reference yield:

: 77-52-1
ursolic acid

: 1351856-48-8
N-(3β-acetoxy-urs-12-en-28-oyl)-1-amino-N-(2-amino-3-phenyl-1-propionyl-)-2-aminoethane

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; dmap

2: oxalyl dichloride / dichloromethane

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / 1,4-dioxane

4: triethylamine / dichloromethane

With pyridine; dmap; oxalyl dichloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2012.02.009

Reference yield:

: 915-79-7,7372-30-7,94482-46-9,105452-47-9,121470-75-5
(3β)-3-acetoxy-urs-12-en-28-carboxylic acid

: 1351856-48-8
N-(3β-acetoxy-urs-12-en-28-oyl)-1-amino-N-(2-amino-3-phenyl-1-propionyl-)-2-aminoethane

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / dichloromethane

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / 1,4-dioxane

3: triethylamine / dichloromethane

With oxalyl dichloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2012.02.009