C₂₃H₂₀INO₆

Base Information

• Chemical Name: C₂₃H₂₀INO₆
• CAS No.: 1455450-13-1
• Molecular Formula: C₂₃H₂₀INO₆
• Molecular Weight: 533.319
• Mol file: 1455450-13-1.mol

Synonyms:C₂₃H₂₀INO₆

Chemical Property of C₂₃H₂₀INO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₂₃H₂₀INO₆

There total 7 articles about C₂₃H₂₀INO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C23H21NO6 (1455450-29-9) → C23H20INO6 (1455450-13-1) + C23H20INO6

Guidance literature:

With iodine; sodium hydrogencarbonate; potassium iodide; In acetonitrile; at 0 - 20 ℃;

DOI:10.1055/s-0033-1340077

Reference yield:

C23H21NO6 → C23H20INO6 (1455450-13-1) + C23H20INO6

Guidance literature:

With iodine; sodium hydrogencarbonate; potassium iodide; In acetonitrile; at 0 ℃; Solvent; Time; Reagent/catalyst; stereoselective reaction;

DOI:10.1039/c3cc44004d

Reference yield:

(2-nitroethenyl)benzene (102-96-5) → C23H20INO6 (1455450-13-1)

Guidance literature:

Multi-step reaction with 3 steps

1: dmap / acetonitrile / 1 h / 20 °C

2: 4-Fluorobenzoic acid; (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine / acetonitrile / 3 h / 20 °C

3: iodine; potassium iodide; sodium hydrogencarbonate / acetonitrile / 0 °C

With (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; dmap; 4-Fluorobenzoic acid; iodine; sodium hydrogencarbonate; potassium iodide; In acetonitrile; 1: |Morita-Baylis-Hillman Alkylation / 2: |Michael Addition;

DOI:10.1039/c3cc44004d

upstream raw materials:

indan-1,2,3-trione hydrate

(2-nitroethenyl)benzene

C₁₄H₁₇NO₃

C₂₃H₂₁NO₆