2,6-dimethylphenyl 3,6-di-O-benzyl-2-azido-2-deoxy-1-β-D-thioglucopyranoside

Base Information

Chemical Name:2,6-dimethylphenyl 3,6-di-O-benzyl-2-azido-2-deoxy-1-β-D-thioglucopyranoside
CAS No.:1200762-83-9
Molecular Formula:C₂₈H₃₁N₃O₄S
Molecular Weight:505.638
Hs Code.:

Synonyms:2,6-dimethylphenyl 3,6-di-O-benzyl-2-azido-2-deoxy-1-β-D-thioglucopyranoside

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Chemical Property of 2,6-dimethylphenyl 3,6-di-O-benzyl-2-azido-2-deoxy-1-β-D-thioglucopyranoside

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Technology Process of 2,6-dimethylphenyl 3,6-di-O-benzyl-2-azido-2-deoxy-1-β-D-thioglucopyranoside

There total 1 articles about 2,6-dimethylphenyl 3,6-di-O-benzyl-2-azido-2-deoxy-1-β-D-thioglucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2,6-dimethylphenyl 2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-1-β-D-thioglucopyranoside

: 1200762-83-9
2,6-dimethylphenyl 3,6-di-O-benzyl-2-azido-2-deoxy-1-β-D-thioglucopyranoside

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; at -5 ℃;
DOI:10.1002/chem.200901119

Reference yield: 60.0%

: 2009-83-8
6-chloro-1-hexanol

: 1200762-83-9
2,6-dimethylphenyl 3,6-di-O-benzyl-2-azido-2-deoxy-1-β-D-thioglucopyranoside

: 1200763-43-4
6-chlorohexyl 2-azido-3,6-di-O-benzyl-2-deoxy-1-β-D-glucopyranoside

Guidance literature:: 6-chloro-1-hexanol; 2,6-dimethylphenyl 3,6-di-O-benzyl-2-azido-2-deoxy-1-β-D-thioglucopyranoside; In dichloromethane; acetonitrile; propiononitrile; at -70 - 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; acetonitrile; propiononitrile; at -70 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/chem.200901119